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P111monil' Laboratories, Inc. <br />2773 Downhill Drive Steamboat Swinas. CO 80487 (800) 334 -5493 <br />Seneca Coal Company ACZ Sample ID. L11909 -01 <br />Project ID: 451129821 Date Sampled: 05106113 08:50 <br />Sample ID: SSC6 Date Received: 05106113 <br />Sample Matrix: Surface Water <br />Inorganic Prep <br />Wet Chemistry <br />- c:a <br />- ar a . <br />0 ' • <br />6 <br />o <br />-• <br />�. <br />Acidity and filter <br />Colorado 5 CCR 1002 - 31.5.31 <br />M200.71200.8 <br />05/08/13 18:36 <br />pmc <br />(Potentially Dissolved) <br />(2009) <br />& Acidification <br />Total Recoverable <br />M200.2 ICP <br />Lab Filtration (glass <br />SOPWC050 <br />05/13/13 17:36 <br />aeb <br />Digestion <br />05/07/13 9:10 <br />dcw <br />fiber filter) <br />Total Recoverable <br />M200.2 JCP -MS <br />Nitrate as N, dissolved <br />05108/13 15:48 <br />sop <br />Digestion <br />mg /L <br />0.02 <br />0.1 <br />05116/13 0:00 <br />talc <br />Nitrate/Nitrite as N, <br />10353.2 - Automated Cadmium <br />Metals Analysis <br />mg /L <br />0.02 <br />0.1 <br />05/07/13 22:59 <br />pjb <br />dissolved <br />Reduction <br />Iron, total recoverable <br />M200.7 ICP <br />0.17 <br />mg/L <br />0.04 <br />0.1 <br />05/15/13 11:14 <br />j)c <br />Manganese, dissolved <br />M200.81CP -MS <br />0.200 + <br />mg /L <br />0.001 <br />0.005 <br />05/14113 3:31 <br />msh <br />Mercury, total <br />M245.1 CVAA <br />U <br />ug /L <br />0.2 <br />1 <br />05/09/1314:41 <br />las <br />Selenium, dissolved <br />M200.8 ICP -MS <br />3.2 <br />ug/L <br />0.2 <br />0.5 <br />05/14/13 18:00 <br />msh <br />Selenium, potentially <br />M200.8 ICP -MS <br />3.4 <br />ug/L <br />0.2 <br />0.5 <br />05/14/13 4:16 <br />pmc <br />dissolved <br />Residue, Non- <br />SM25400 <br />Selenium, total <br />M200.8 ICP -MS <br />3.6 <br />ugfL <br />0.2 <br />0.5 <br />05/10/13 20:00 <br />pmc <br />recoverable <br />./ <br />@105C <br />Wet Chemistry <br />- c:a <br />- ar a . <br />0 ' • <br />6 <br />o <br />-• <br />�. <br />Lab Filtration (0.45um) <br />M200.71200.8 <br />05/08/13 12:25 <br />las <br />& Acidification <br />Lab Filtration (glass <br />SOPWC050 <br />05/07/13 9:10 <br />dcw <br />fiber filter) <br />Nitrate as N, dissolved <br />Calculation: NO3NO2 minus NO2 <br />0.50 <br />mg /L <br />0.02 <br />0.1 <br />05116/13 0:00 <br />talc <br />Nitrate/Nitrite as N, <br />10353.2 - Automated Cadmium <br />0.50 <br />mg /L <br />0.02 <br />0.1 <br />05/07/13 22:59 <br />pjb <br />dissolved <br />Reduction <br />Nitrite as N, dissolved <br />M353.2 - Automated Cadmium <br />U <br />mg/L <br />0.01 <br />0.05 <br />05/07113 22:59 <br />pjb <br />Reduction <br />Nitrogen, ammonia <br />M350.1 - Automated Phenate <br />U <br />mg /L <br />0.05 <br />0.5 <br />05/13/13 13:46 <br />lhb <br />Residue, Filterable <br />SM2540C <br />3080 <br />mg /L <br />10 <br />20 <br />05/07/13 15:37 <br />dcw <br />(fDS) @180C <br />Residue, Non- <br />SM25400 <br />U <br />mg/L <br />5 <br />20 <br />05/07113 16:12 <br />mss3 <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D51"2 - Turbidimehic <br />2000 <br />' <br />mg /L <br />100 <br />500 <br />05/15/13 9:47 <br />bsu <br />Sulfide as S <br />SM4500S2 -D <br />U <br />mg/L <br />0.02 <br />0.1 <br />05107/1311:31 <br />Ijr <br />REPIN.02.06,05.01 "Please refer to Qualifier Reports for details. <br />Page 2 of 30 <br />