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ACZ Laboratories, Inc. <br />Star Mine Operations LLC ACZ Project ID: L12889 <br />Alkalinity as CaCO3 <br />• <br />1.964 <br />SM2320B - Titration <br />• <br />98.2 <br />WG3466941CV <br />ICV <br />06/29/1310:44 <br />M Limit Qual <br />WG346393 <br />ICB <br />06/29/1310:50 <br />WG3467681CV <br />ICV <br />07/01/1318.46 <br />11130510 -1 <br />2 <br />WG346643LFB <br />WG346393PBW1 PBW <br />06/25/1317:26 <br />101.4 <br />95 <br />14.7 <br />mg/L <br />ICB <br />-20 <br />20 <br />WG346393LCSW2 LCSW <br />06/25/1317:47 <br />WC130625- <br />820.0001 <br />745.8 <br />mg/L <br />91 <br />90 <br />110 <br />WG346393LCSW5 LCSW <br />06/25/13 21:05 <br />WC130625- <br />820.0001 <br />784.9 <br />mg/L <br />95.7 <br />90 <br />110 <br />WG346393PBW2 PBW <br />06/25/13 21:13 <br />07/01/13 20:09 <br />11130621 -2 <br />2.9 <br />mg/L <br />.978 <br />-20 <br />20 <br />WG346393LCSW8 LCSW <br />06/26113 0:02 <br />WC130625- <br />820.0001 <br />772.9 <br />mg/L <br />94.3 <br />90 <br />110 <br />WG346393PBW3 PBW <br />06/26/13 0:10 <br />85 <br />115 1.22 20 <br />31 <br />mg/L <br />-20 <br />20 <br />L12910 -01DUP DUP <br />06/26/131:40 <br />279 <br />279.9 <br />mg/L <br />WG3467741CV <br />ICV <br />0.3 20 <br />WG346393LCSWll LCSW <br />06/26/13 3:26 <br />WC13G625- <br />820.0001 <br />775.5 <br />mg/L <br />94.6 <br />90 <br />110 <br />WG346393PBW4 PBW <br />06/26/13 3:35 <br />2.6 <br />mg/L <br />mg/L <br />-20 <br />20 <br />WG346393LCSW14 LCSW <br />06 /26113 6:43 <br />WC13O625- <br />820.0001 <br />797.6 <br />mg/L <br />97.3 <br />90 <br />110 <br />Aluminum, dissolved <br />M200.7 ICP <br />WG346768 <br />1.964 <br />mg /L <br />98.2 <br />WG3466941CV <br />ICV <br />06/29/1310:44 <br />11130514 -1 <br />WG346694ICB <br />ICB <br />06/29/1310:50 <br />WG3467681CV <br />ICV <br />07/01/1318.46 <br />11130510 -1 <br />2 <br />WG346643LFB <br />2.027 <br />mg/L <br />101.4 <br />95 <br />105 <br />WG346768ICB <br />ICB <br />07/01/1318:52 <br />LFMD <br />06/29/1312:08 <br />11130621 -2 <br />U <br />mg/L <br />U <br />-0.09 <br />0.09 <br />WG346768LFB <br />LFB <br />07/01/1319:05 <br />11130621 -2 <br />1.0011 <br />.01 <br />1.024 <br />mg/L <br />102.3 <br />85 <br />115 <br />L12882 -03AS <br />AS <br />07/01/13 20:09 <br />11130621 -2 <br />1.0011 <br />U <br />.978 <br />mg/L <br />97.7 <br />85 <br />115 <br />L12882 -03ASD <br />ASD <br />07/01113 20:19 <br />11130621 -2 <br />1.0011 <br />U <br />.99 <br />mg/L <br />98.9 <br />85 <br />115 1.22 20 <br />WG346774 <br />WG3467741CV <br />ICV <br />07/01/13 20.54 <br />11130510 -1 <br />2 <br />2.031 <br />mg/L <br />101.6 <br />95 <br />105 <br />WG346774ICB <br />ICB <br />07/01/13 20.59 <br />U <br />mg/L <br />-0.09 <br />0.09 <br />WG346774LFB <br />LFB <br />07/01/13 21:12 <br />11130621 -2 <br />1.0011 <br />1.037 <br />mg/L <br />103.6 <br />85 <br />115 <br />L12888-OIAS <br />AS <br />07/01/13 22:04 <br />11130621 -2 <br />1.0011 <br />U <br />1.047 <br />mg/L <br />104.6 <br />85 <br />115 <br />L12888 -01ASD <br />ASD <br />07/01/13 22:07 <br />11130621 -2 <br />1.0011 <br />U <br />1.056 <br />mg/L <br />105.5 <br />85 <br />115 0.86 20 <br />Aluminum, total <br />M200.7 ICP <br />WG346694 <br />1.964 <br />mg /L <br />98.2 <br />WG3466941CV <br />ICV <br />06/29/1310:44 <br />11130514 -1 <br />WG346694ICB <br />ICB <br />06/29/1310:50 <br />130 1.91 20 <br />WG346643LRB <br />LRB <br />06/29/1311:02 <br />102.2 <br />WG346643LFB <br />LFB <br />06/29/1311:05 <br />11130621 -2 <br />L12888 -01LFM <br />LFM <br />06/29/1312:05 <br />11130621 -2 <br />L12888- 01LFMD <br />LFMD <br />06/29/1312:08 <br />11130621 -2 <br />2 <br />1.964 <br />mg /L <br />98.2 <br />-0.066 <br />U <br />mg /L <br />115 <br />70 <br />U <br />mg/L <br />130 1.91 20 <br />1.0011 <br />1.023 <br />mg /L <br />102.2 <br />1.0011 <br />.08 1.16 <br />mg /L <br />107.9 <br />1.0011 <br />.08 1.138 <br />mg/L <br />105.7 <br />95 <br />105 <br />-0.09 <br />0.09 <br />-0.066 <br />0.066 <br />85 <br />115 <br />70 <br />130 <br />70 <br />130 1.91 20 <br />Antimony, dissolved <br />M200.8 ICP -MS <br />• <br />WG346889 <br />WG3468891CV ICV <br />07/03/13 3:44 <br />MS130416 -2 <br />.02 <br />.02193 <br />mg/L <br />109.7 <br />90 <br />110 <br />WG3468891CB ICB <br />07/03/13 3:47 <br />U <br />mg/L <br />- 0.0012 <br />0.0012 <br />WG346889LFB LFB <br />07/03/13 3:50 <br />MS130614 -1 <br />.01 <br />.0099 <br />mg/L <br />99 <br />85 <br />115 <br />L12888 -04AS AS <br />07/03/13 4:14 <br />MS130614 -1 <br />01 <br />U .0094 <br />mg /L <br />94 <br />70 <br />130 <br />L12888 -04ASD ASD <br />07/03/13 4:18 <br />MS130614 -1 <br />.01 <br />U .00961 <br />mg/L <br />96.1 <br />70 <br />130 2.21 20 <br />REPIN.01.06.05.01 Page 12 of 32 <br />