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ACZ Laboratories, Inc. <br />n770 n­'_. ;ll n.:..,. 0.....- J.....♦ 0_.f --- nn on'07 /onnl 09A =An, <br />Star Mine Operations LLC <br />Project ID: <br />Sample ID: SW -1 <br />ACZ Sample ID: <br />L12888 -01 <br />Date Sampled: <br />06120113 10:00 <br />Date Received: <br />06171113 <br />Sample Matrix: <br />Surface Water <br />Sodium, total <br />M200.7 ICP <br />1 <br />1.5 <br />B <br />mg /L <br />0.3 <br />2 <br />06/29/13 12:02 <br />j c <br />Thallium, dissolved <br />M200.8 ICP -MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />07/03/13 4:01 <br />msh <br />Thallium, total <br />M200.8 ICP-MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />07/02/13 21:09 <br />msh <br />Uranium, dissolved <br />M200.8 ICP-MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />07/03/13 4:01 <br />msh <br />Uranium, total <br />M200.8 ICP-MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />07/02/13 21:09 <br />msh <br />Vanadium, dissolved <br />M200.7ICP <br />1 <br />U <br />mg /L <br />0.005 <br />0.03 <br />07/01/13 22:01 <br />& <br />Vanadium, total <br />M200.7 ICP <br />1 <br />U <br />mg /L <br />0.005 <br />0.03 <br />06/29/13 12:02 <br />he <br />Zinc, dissolved <br />M200.71CP <br />1 <br />0.20 <br />mg /L <br />0.01 <br />0.05 <br />07/01/1322:01 <br />he <br />Zinc, total <br />M200.7 ICP <br />1 <br />0.22 <br />mg /L <br />0.01 <br />0.05 <br />06/29/13 12:02 <br />he <br />Wet Chemistry <br />Parameter <br />EPA it Dilution <br />Result <br />! <br />a: <br />MDL <br />PQL <br />!. <br />Alkalinity as CaCC3 <br />SM23208- Titration <br />Bicarbonate as <br />1 <br />41 <br />mg /L <br />2 <br />20 <br />06/26/13 0:00 <br />khw <br />CaCO3 <br />Carbonate as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />06/26113 0:00 <br />khw <br />Hydro )dde as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />06/26/13 0:00 <br />khw <br />Total Alkalinity <br />1 <br />41 <br />mg /L <br />2 <br />20 <br />06/26/13 0:00 <br />khw <br />Cation -Anion Balance <br />calculation <br />Cation -Anion Balance <br />-14.3 <br />% <br />07/12/13 0:00 <br />talc <br />Sum of Anions <br />1.6 <br />meq /L <br />0.1 <br />0.5 <br />07/12/13 0:00 <br />talc <br />Sum of Cations <br />1.2 <br />meq /L <br />0.1 <br />0.5 <br />07/12/13 0:00 <br />talc <br />Chloride <br />SM4500CI -E <br />1 <br />U <br />* mg /L <br />1 <br />5 <br />07/03/1316:12 <br />mpb <br />Conductivity @25C <br />SM251OB <br />1 <br />130 <br />umhos /cm <br />1 <br />10 <br />06/26/13 0:19 <br />khw <br />Cyanide, total <br />M335.4- Colorimetricw /distillation <br />0.5 <br />U <br />* mg /L <br />0.003 <br />0.01 <br />07/02/1315:28 <br />mpb <br />Cyanide, WAD <br />SM4500 -CN I- Colorimetric <br />0.5 <br />U <br />mg /L <br />0.003 <br />0.01 <br />07/02/13 16:24 <br />mpb <br />w/ distillation <br />Fluoride <br />SM450OF -C <br />1 <br />0.1 <br />B <br />mg /L <br />0.1 <br />0.5 <br />06/28/1313:01 <br />abm <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />57 <br />mg /L <br />1 <br />7 <br />07/12/13 0:00 <br />talc <br />Lab Filtration (0.45um) <br />M200.71200.8 <br />1 <br />06/27/13 12:00 <br />scp <br />& Acidification <br />Lab Filtration (glass <br />SOPWC050 <br />1 <br />06/25/13 12:25 <br />khw <br />fiber filter) <br />Nitrate /Nitrite as N <br />M353.2 - H2SO4 preserved <br />1 <br />0.31 <br />mg /L <br />0.02 <br />0.1 <br />07/03/13 0:49 <br />pjb <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />7.8 <br />H <br />units <br />0.1 <br />0.1 <br />06/26/13 0:00 <br />khw <br />pH measured at <br />1 <br />20.0 <br />C <br />0.1 <br />0.1 <br />06/26/13 0:00 <br />khw <br />Phosphorus, ortho <br />M365.1- Automated Ascorbic Acid <br />1 <br />0.01 <br />B <br />mg /L <br />0.01 <br />0.05 <br />06/21/13 22:00 <br />pjb <br />dissolved <br />Residue, Filterable <br />SM2540C <br />1 <br />70 <br />* mg /L <br />10 <br />20 <br />06/26/13 10:57 <br />dcw <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />U <br />* mg /L <br />5 <br />20 <br />06/27/13 12:02 <br />mss3 <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516.02- Turbidimetnc <br />1 <br />38.0 <br />mg /L <br />1 <br />5 <br />07/02/1318:06 <br />mpb <br />TDS (calculated) <br />calculation <br />90 <br />mg /L <br />10 <br />50 <br />07/12/13 0:00 <br />talc <br />TDS (ratio - <br />calculation <br />0.78 <br />07/12/13 0:00 <br />talc <br />measured /calculated) <br />REPIN.02.06.05.01 * P /ease refer to Qualifier Reports for details <br />Page 4 of 45 <br />