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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Sonnas_ CO 80487 (800) <br />Star Mine Operations LLC <br />Project ID: <br />Sample ID: MW -4 <br />Wet Chemistry <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />L12887 -04 <br />06120113 08:40 <br />06/21/13 <br />Waste Water <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 9 of 29 <br />• <br />w e <br />Inits <br />-I&IJIL <br />eQL <br />r• <br />Alkalinity as CaCO3 <br />SM2320B - Titration <br />Bicarbonate as <br />1 <br />47 <br />mg /L <br />2 <br />20 <br />06/25/13 0:00 <br />khw <br />CaCO3 <br />Carbonate as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />06/25/13 0:00 <br />khw <br />Hydroxide as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />06/25/13 0:00 <br />khw <br />Total Alkalinity <br />1 <br />47 <br />mg /L <br />2 <br />20 <br />06/25/13 0:00 <br />khw <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />-7.7 <br />% <br />07/12/13 0:00 <br />talc <br />Sum of Anions <br />1.4 <br />meq/L <br />0.1 <br />0.5 <br />07/12/13 0:00 <br />talc <br />Sum of Cations <br />1.2 <br />meq/L <br />0.1 <br />0.5 <br />07/12/13 0:00 <br />talc <br />Chloride <br />SM4500CI -E <br />1 <br />U <br />mg /L <br />1 <br />5 <br />07/03/1316:12 <br />mpb <br />Conductivity @25C <br />SM251OB <br />1 <br />144 <br />umhos /cm <br />1 <br />10 <br />06/25/13 23:33 <br />khw <br />Cyanide, total <br />M335.4- Colonmetncw /distillation <br />0.5 <br />U * <br />mg /L <br />0.003 <br />0.01 <br />07/02/13 15:24 <br />mpb <br />Cyanide, WAD <br />SM4500 -CN I- Colorimetric <br />0.5 <br />U <br />mg /L <br />0.003 <br />0.01 <br />07/02/13 14:48 <br />mpb <br />w/ distillation <br />Fluoride <br />SM450OF -C <br />1 <br />U <br />mg /L <br />0.1 <br />0.5 <br />06/28/1312:52 <br />abm <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />54 <br />mg /L <br />1 <br />7 <br />07/12/13 0:00 <br />talc <br />Lab Filtration (0.45um) <br />M200.7/200.8 <br />1 <br />06/27/13 12:00 <br />scp <br />& Acidification <br />Lab Filtration (glass <br />SOPWC050 <br />1 <br />06/25/13 12:21 <br />khw <br />fiber filter) <br />Nitrate /Nitrite as N <br />M353.2 - H2SO4 preserved <br />1 <br />0.23 <br />mg /L <br />0.02 <br />0.1 <br />07/03/13 0:46 <br />pjb <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />8.1 <br />H <br />units <br />0.1 <br />0.1 <br />06/25/13 0:00 <br />khw <br />pH measured at <br />1 <br />20.0 <br />C <br />0.1 <br />0.1 <br />06/25/13 0:00 <br />khw <br />Phosphorus, ortho <br />M365.1- Automated Ascorbic AGd <br />1 <br />0.01 <br />B • <br />mg /L <br />0.01 <br />0.05 <br />06/21/1321:58 <br />pjb <br />dissolved <br />Residue, Filterable <br />SM2540C <br />1 <br />80 <br />mg /L <br />10 <br />20 <br />06/26/13 10:52 <br />dcw <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />U <br />mg /L <br />5 <br />20 <br />06/26/13 11:03 <br />mss3 <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516- 02- Turbidimetnc <br />1 <br />23.0 <br />mg /L <br />1 <br />5 <br />07/02/1318:04 <br />mpb <br />TDS (calculated) <br />Calculation <br />80 <br />mg /L <br />10 <br />50 <br />07/12/13 0:00 <br />talc <br />TDS (ratio - <br />Calculation <br />1.00 <br />07/12/13 0:00 <br />talc <br />measured /calculated) <br />For Cadmium by ICPMS, <br />the value in the MDL <br />field is the client's requested reporting limit. <br />A "U" qualifier denotes cadmium was not detected above this level. <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 9 of 29 <br />