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■ 72 wwwtmralab.com Helena. W 677472 -0711 • Billings, W 800 -735 -4489 • Casper, WY 888- 235 -0515 <br />. L"i�n MdybaiFrc�lancrsJnc. felt Gillette, WY 866.686 -7175 • Rapid City, SO 088 -672 -1225 • College Station, TX 888 -690 -2216 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation Report Date: 05/01/13 <br />Project: Schwartz SW 4/03/13 S26861 Work Order: C13040193 <br />Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.7 <br />6 Interference Check Sample AB <br />Aluminum <br />481 mg /L <br />Analytical Run: ICP4- C_130408A <br />Sample ID: ICV <br />6 Initial Calibration Verification Standard <br />0.10 <br />Iron <br />04/08/13 12:13 <br />Aluminum <br />4.97 mg /L <br />0.10 <br />99 <br />95 <br />105 <br />Boron <br />1.03 mg /L <br />0.10 <br />103 <br />95 <br />105 <br />Iron <br />5.00 mg /L <br />0.030 <br />100 <br />95 <br />105 <br />Manganese <br />4.90 mg /L <br />0.010 <br />98 <br />95 <br />105 <br />Molybdenum <br />1.01 mg /L <br />0.10 <br />101 <br />95 <br />105 <br />Zinc <br />0.998 mg /L <br />0.010 <br />100 <br />95 <br />105 <br />Sample ID: ICSA <br />6 Interference Check Sample A <br />0.003 mg /L <br />0.001 <br />04/08/13 12:27 <br />Aluminum <br />474 mg /L <br />0.10 <br />95 <br />80 <br />120 <br />Boron <br />0.00137 mg /L <br />0.10 <br />0.10 <br />104 <br />85 115 <br />Iron <br />174 mg /L <br />0.030 <br />87 <br />80 <br />120 <br />Manganese <br />0.00356 mg /L <br />0.010 <br />0.030 <br />104 <br />85 115 <br />Molybdenum <br />- 0.000210 mg /L <br />0.10 <br />0.010 <br />102 <br />85 115 <br />Zinc <br />0.0169 mg /L <br />0.010 <br />0.10 <br />102 <br />85 115 <br />Sample ID: ICSAB <br />6 Interference Check Sample AB <br />Aluminum <br />481 mg /L <br />0.10 <br />Boron <br />- 0.00457 mg /L <br />0.10 <br />Iron <br />175 mg /L <br />0.030 <br />Manganese <br />0.453 mg /L <br />0.010 <br />Molybdenum <br />- 0.000750 mg /L <br />0.10 <br />Zinc <br />0.860 mg /L <br />0.010 <br />96 80 120 <br />87 80 120 <br />91 80 120 <br />86 80 120 <br />04/08/13 12:31 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />Page 10 of 25 <br />Method: E200.7 <br />Batch: 37059 <br />Sample ID: MB -37059 <br />6 Method Blank <br />Run: ICP4- C_130408A <br />04/08/13 15:58 <br />Aluminum <br />0.01 mg /L <br />0.009 <br />Boron <br />ND mg /L <br />0.002 <br />Iron <br />ND mg /L <br />0.002 <br />Manganese <br />ND mg /L <br />0.0010 <br />Molybdenum <br />ND mg /L <br />0.003 <br />Zinc <br />0.003 mg /L <br />0.001 <br />Sample ID: LCS3 -37059 <br />6 Laboratory Control Sample <br />Run: ICP4- C_130408A <br />04/08/13 16:02 <br />Aluminum <br />2.6 mg /L <br />0.10 <br />104 <br />85 115 <br />Boron <br />0.52 mg /L <br />0.10 <br />104 <br />85 115 <br />Iron <br />2.6 mg /L <br />0.030 <br />104 <br />85 115 <br />Manganese <br />2.5 mg /L <br />0.010 <br />102 <br />85 115 <br />Molybdenum <br />0.51 mg /L <br />0.10 <br />102 <br />85 115 <br />Zinc <br />0.51 mg /L <br />0.010 <br />101 <br />85 115 <br />Sample ID: C13040184 -001 BMS3 <br />6 Sample Matrix Spike <br />Run: ICP4- C_130408A <br />04/08/13 16:54 <br />Aluminum <br />2.6 mg /L <br />0.10 <br />100 <br />70 130 <br />Boron <br />0.63 mg /L <br />0.10 <br />99 <br />70 130 <br />Iron <br />2.6 mg /L <br />0.030 <br />99 <br />70 130 <br />Manganese <br />2.4 mg /L <br />0.010 <br />97 <br />70 130 <br />Molybdenum <br />0.48 mg /L <br />0.10 <br />96 <br />70 130 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />Page 10 of 25 <br />