Laserfiche WebLink
wwwtmgylab.com r Helena. MT 877- 472 -0711 • Billings, MT 800 -735 -4489 • Casper, WY 888- 235 -0515 <br />AW#",rreee nc Gillette, W <br />S*W 1852 Y 866- 686 -7175 • Rapid City, SD 688- 672 -1225 0 College Station, TX 888 - 680 -2210 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation Report Date: 05/01/13 <br />Project: Schwartz SW 4/03/13 S26860 Work Order: C13040198 <br />Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.8 <br />Sample Matrix Spike <br />Run: ICPMS2- C_130411A 04/12/13 01:22 <br />Aluminum <br />0.0957 <br />Batch: R172395 <br />Analytical Run: ICPMS2- C_130411A <br />Sample ID: ICV <br />9 Initial Calibration Verification <br />Standard <br />0.0010 105 70 130 <br />Run: ICPMS2- C_130411A 04/11/13 11:02 <br />04/11/13 10:36 <br />Aluminum <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Antimony <br />0.0514 <br />mg /L <br />0.0010 <br />103 <br />90 <br />110 <br />Copper <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Manganese <br />0.0500 <br />mg /L <br />0.0010 <br />100 <br />90 <br />110 <br />Molybdenum <br />0.0498 <br />mg /L <br />0.0010 <br />100 <br />90 <br />110 <br />Silver <br />0.0200 <br />mg /L <br />0.0010 <br />100 <br />90 <br />110 <br />Thallium <br />0.0498 <br />mg /L <br />0.0010 <br />100 <br />90 <br />110 <br />Uranium <br />0.0500 <br />mg /L <br />0.00030 <br />100 <br />90 <br />110 <br />Zinc <br />0.0494 <br />mg /L <br />0.0010 <br />99 <br />90 <br />110 <br />Method: E200.8 <br />Sample Matrix Spike <br />Run: ICPMS2- C_130411A 04/12/13 01:22 <br />Aluminum <br />0.0957 <br />Batch: R172395 <br />Sample ID: LRB <br />9 Method Blank <br />0.105 <br />mg /L <br />0.0010 105 70 130 <br />Run: ICPMS2- C_130411A 04/11/13 11:02 <br />Aluminum <br />ND <br />mg /L <br />0.001 <br />1.93 <br />mg /L <br />Antimony <br />8E -05 <br />mg /L <br />6E -05 <br />0.0010 105 70 130 <br />Silver <br />Copper <br />ND <br />mg /L <br />0.0001 <br />0.104 <br />mg /L <br />Manganese <br />ND <br />mg /L <br />2E -05 <br />0.00030 70 130 A <br />Zinc <br />Molybdenum <br />ND <br />mg /L <br />4E -05 <br />Silver <br />ND <br />mg /L <br />5E -05 <br />A - The analyte level was greater than four times the spike level. In <br />Thallium <br />ND <br />mg /L <br />9E -06 <br />Uranium <br />0.0001 <br />mg /L <br />1 E -05 <br />Zinc <br />0.001 <br />mg /L <br />0.0006 <br />Sample ID: LFB <br />9 Laboratory Fortified <br />Blank <br />Run: ICPMS2- C_130411A 04/11/13 11:05 <br />Aluminum <br />0.0485 <br />mg /L <br />0.0010 <br />97 <br />85 115 <br />Antimony <br />0.0496 <br />mg /L <br />0.0010 <br />99 <br />85 115 <br />Copper <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />85 115 <br />Manganese <br />0.0495 <br />mg /L <br />0.0010 <br />99 <br />85 115 <br />Molybdenum <br />0.0493 <br />mg /L <br />0.0010 <br />99 <br />85 115 <br />Silver <br />0.0192 <br />mg /L <br />0.0010 <br />96 <br />85 115 <br />Thallium <br />0.0501 <br />mg /L <br />0.0010 <br />100 <br />85 115 <br />Uranium <br />0.0502 <br />mg /L <br />0.00030 <br />100 <br />85 115 <br />Zinc <br />0.0518 <br />mg /L <br />0.0010 <br />101 <br />85 115 <br />Sample ID: C13040217- 003BMS4 9 <br />Sample Matrix Spike <br />Run: ICPMS2- C_130411A 04/12/13 01:22 <br />Aluminum <br />0.0957 <br />mg /L <br />0.030 96 70 130 <br />Antimony <br />0.105 <br />mg /L <br />0.0010 105 70 130 <br />Copper <br />0.0961 <br />mg /L <br />0.0050 93 70 130 <br />Manganese <br />1.93 <br />mg /L <br />0.0010 70 130 A <br />Molybdenum <br />0.136 <br />mg /L <br />0.0010 105 70 130 <br />Silver <br />0.0346 <br />mg /L <br />0.0010 87 70 130 <br />Thallium <br />0.104 <br />mg /L <br />0.00050 104 70 130 <br />Uranium <br />0.551 <br />mg /L <br />0.00030 70 130 A <br />Zinc <br />0.102 <br />mg /L <br />0.010 84 70 130 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />A - The analyte level was greater than four times the spike level. In <br />accordance with the method % recovery is not calculated. <br />ND - Not detected at the reporting limit. <br />MDC - Minimum detectable concentration <br />Page 13 of 25 <br />