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AOZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Spnngs, CO 80487 (800) 334 -5493 <br />Golder Associates ACZ Project ID: L11197 <br />L11197 -01 WG340820 Manganese, dissolved <br />M200 7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level The recovery of the associated control sample (LCS <br />or LFB) was acceptable <br />WG341037 Chloride <br />M300 0 - Ion Chromatography <br />DC <br />Sample required dilution Non - target analyte exceeded <br />calibration range <br />WG341070 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />WG340929 pH <br />SM4500H+ B <br />ZW <br />Method deviation The sample was centrifuged prior to <br />analysis due to high solid content <br />WG340923 Residue, Filterable (TDS) @180C <br />SM2540C <br />ZO <br />Concentration is based on a final residue greater than 200 <br />mg <br />WG340929 Total Alkalinity <br />SM2320B - Titration <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL) <br />SM2320B - Titration <br />ZW <br />Method deviation The sample was centrifuged prior to <br />analysis due to high solid content <br />L11197 -02 WG340820 Manganese, dissolved <br />M200 7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level The recovery of the associated control sample (LCS <br />or LFB) was acceptable <br />WG341070 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />WG340929 pH <br />SM4500H+ B <br />ZW <br />Method deviation The sample was centrifuged prior to <br />analysis due to high solid content <br />WG340923 Residue, Filterable (TDS) @180C <br />SM2540C <br />ZO <br />Concentration is based on a final residue greater than 200 <br />mg <br />WG341037 Sulfate <br />M300 0 - Ion Chromatography <br />DC <br />Sample required dilution Non - target analyte exceeded <br />calibration range <br />WG340929 Total Alkalinity <br />SM2320B - Titration <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />SM2320B - Titration <br />ZW <br />Method deviation The sample was centrifuged prior to <br />analysis due to high solid content <br />L11197 -03 WG340820 Barium, dissolved <br />M200 7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level The recovery of the associated control sample (LCS <br />or LFB) was acceptable <br />WG341070 Fluoride <br />SM450OF -C <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />WG341153 Sulfate <br />M300 0 - Ion Chromatography <br />DC <br />Sample required dilution Non - target analyte exceeded <br />calibration range <br />M300 0 - Ion Chromatography <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />WG340929 Total Alkalinity <br />SM2320B - Titration <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL) <br />REPAID 15.06 05.01 <br />Page 20 of 26 <br />