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AC3Z <br />Laboratories, Inc. <br />°...m.• ..... g j; <br />Acidify and filter <br />2773 Downhill Drive Steamboat Spnngs, CO 80487 (800) 334 -5493 <br />02/07/13 16-00 <br />Iron, total recoverable <br />(Potentially Dissolved) <br />(2009) <br />B mg/L <br />scp <br />Total Recoverable <br />Seneca Coal Company <br />ACZ Sample ID: <br />L10485-04 <br />Project ID: 450855601 <br />Date Sampled: <br />02104113 11:30 <br />Sample ID: NPDES4 <br />Date Received: <br />02104113 <br />02/07113 17:22 <br />Sample Matrix: <br />Surface Water <br />Inorganic Prep <br />Metals Analysis <br />°...m.• ..... g j; <br />Acidify and filter <br />Colorado 5 CCR 1002-31.5.31 <br />02/07/13 16-00 <br />Iron, total recoverable <br />(Potentially Dissolved) <br />(2009) <br />B mg/L <br />scp <br />Total Recoverable <br />M200.2 ICP -MS <br />02/07113 12:24 <br />M200.8 ICP-MS <br />Digestion <br />ug/L <br />0.1 <br />scp <br />Total Recoverable <br />M200.2 ICP <br />02/07113 17:22 <br />flc <br />Digestion <br />h <br />Metals Analysis <br />Wet Chemistry <br />Lab Filtration (glass SOPWC050 <br />fiber filter) <br />Residue, Filterable SM2540C 4210 <br />(TDS) @180C <br />02/05/13 14.16 Ijr <br />mg/L 10 20 02/05/1315:41 Ijr <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 6 of 12 <br />Iron, total recoverable <br />M200.7 ICP <br />0.2 <br />B mg/L <br />0.1 <br />0.3 02/08/13 13:52 <br />jjc <br />Selenium, potentially <br />M200.8 ICP-MS <br />1 <br />ug/L <br />0.1 <br />0.3 02/15/13 2:55 <br />scp/ms <br />dissolved <br />h <br />Selenium, total <br />M200.8 ICP-MS <br />1 <br />ug/L <br />0.5 <br />1 02/08/13 0:56 <br />pmc <br />recoverable <br />Wet Chemistry <br />Lab Filtration (glass SOPWC050 <br />fiber filter) <br />Residue, Filterable SM2540C 4210 <br />(TDS) @180C <br />02/05/13 14.16 Ijr <br />mg/L 10 20 02/05/1315:41 Ijr <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 6 of 12 <br />