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Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />Page 8 of 19 <br />WWWO erDIab.com <br />Helena, W 877 -472 -0711 • Billings, W 800 -735 -4489 • Casper, WY 868 -235 -0515 <br />° e W <br />Gillette, <br />J <br />WY 866- 686 -7175 • <br />Rapid City, SD 888 -672 -1225 • College Station, TX 888 -690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY <br />Branch <br />Client: Cotter Corporation <br />Report Date: <br />02/06/13 <br />Project: Schwartz GW 1/22/13 SSTF: S26783 <br />Work Order: <br />C13010694 <br />[Analy te Count Result <br />Units <br />RL <br />%REC <br />Low Limit <br />High Limit RPD <br />RPDLimit Qual <br />Method: E200.7 <br />Batch: 36369 <br />Sample ID: C1 3010692-001 AMS3 <br />5 Sample Matrix Spike <br />Run: ICP2- C_130125A <br />01/25/13 20:34 <br />Aluminum <br />2.58 <br />mg /L <br />0.030 <br />103 <br />70 <br />130 <br />Copper <br />0.529 <br />mg /L <br />0.0050 <br />102 <br />70 <br />130 <br />Iron <br />2.59 <br />mg /L <br />0.030 <br />103 <br />70 <br />130 <br />Manganese <br />2.54 <br />mg /L <br />0.0010 <br />102 <br />70 <br />130 <br />Zinc <br />0.519 <br />mg /L <br />0.010 <br />100 <br />70 <br />130 <br />Sample ID: C13010692 -001AMSD <br />5 Sample Matrix Spike Duplicate <br />Run: ICP2- C_130125A <br />01/25/13 21:18 <br />Aluminum <br />2.58 <br />mg /L <br />0.030 <br />102 <br />70 <br />130 0.2 <br />20 <br />Copper <br />0.526 <br />mg /L <br />0.0050 <br />101 <br />70 <br />130 0.5 <br />20 <br />Iron <br />2.60 <br />mg /L <br />0.030 <br />104 <br />70 <br />130 0.6 <br />20 <br />Manganese <br />2.56 <br />mg /L <br />0.0010 <br />102 <br />70 <br />130 0.6 <br />20 <br />Zinc <br />0.528 <br />mg /L <br />0.010 <br />101 <br />70 <br />130 1.6 <br />20 <br />Method: E200.7 <br />Batch: R169589 <br />Sample ID: MS- 130125A <br />5 Method Blank <br />Run: ICP2- C_130125A <br />01/25/13 14:04 <br />Calcium <br />ND <br />mg /L <br />0.06 <br />Iron <br />ND <br />mg /L <br />0.001 <br />Magnesium <br />ND <br />mg /L <br />0.03 <br />Potassium <br />ND <br />mg /L <br />0.06 <br />Sodium <br />ND <br />mg /L <br />0.03 <br />Sample ID: LFB- 130125A <br />5 Laboratory Fortified <br />Blank <br />Run: ICP2- C_130125A <br />01/25/13 14:08 <br />Calcium <br />48.9 <br />mg /L <br />0.50 <br />98 <br />85 <br />115 <br />Iron <br />0.997 <br />mg /L <br />0.030 <br />100 <br />85 <br />115 <br />Magnesium <br />49.3 <br />mg /L <br />0.50 <br />99 <br />85 <br />115 <br />Potassium <br />45.8 <br />mg /L <br />0.50 <br />92 <br />85 <br />115 <br />Sodium <br />49.7 <br />mg /L <br />0.50 <br />99 <br />85 <br />115 <br />Sample ID: C13010694 -001CMS2 <br />5 Sample Matrix Spike <br />Run: ICP2- C_130125A <br />01/25/13 19:46 <br />Calcium <br />111 <br />mg /L <br />1.0 <br />92 <br />70 <br />130 <br />Iron <br />0.978 <br />mg /L <br />0.030 <br />93 <br />70 <br />130 <br />Magnesium <br />65.6 <br />mg /L <br />1.0 <br />95 <br />70 <br />130 <br />Potassium <br />50.6 <br />mg /L <br />1.0 <br />94 <br />70 <br />130 <br />Sodium <br />69.6 <br />mg /L <br />1.0 <br />104 <br />70 <br />130 <br />Sample ID: 013010694- 001CMSD <br />5 Sample Matrix Spike Duplicate <br />Run: ICP2- C_130125A <br />01/25/13 19:50 <br />Calcium <br />110 <br />mg /L <br />1.0 <br />90 <br />70 <br />130 0.6 <br />20 <br />Iron <br />0.981 <br />mg /L <br />0.030 <br />93 <br />70 <br />130 0.3 <br />20 <br />Magnesium <br />66.8 <br />mg /L <br />1.0 <br />97 <br />70 <br />130 1.8 <br />20 <br />Potassium <br />50.7 <br />mg /L <br />1.0 <br />95 <br />70 <br />130 0.4 <br />20 <br />Sodium <br />68.0 <br />mg /L <br />1.0 <br />101 <br />70 <br />130 2.2 <br />20 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />Page 8 of 19 <br />