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ENERGY <br />Client: Cotter Corporation <br />Project: Schwartz GW 10/25/2012 S26616 <br />Analyte <br />Method: E200.7 <br />Sample ID: ICV <br />Boron <br />Calcium <br />Iron <br />Magnesium <br />Potassium <br />Sodium <br />Zinc <br />Sample ID: ICSA <br />Boron <br />Calcium <br />Iron <br />Magnesium <br />Potassium <br />Sodium <br />Zinc <br />Sample ID: ICSAB <br />Boron <br />Calcium <br />Iron <br />Magnesium <br />Potassium <br />Sodium <br />Zinc <br />Method: E200.7 <br />Sample ID: MB -35564 <br />Iron <br />Zinc <br />Sample ID: <br />Iron <br />Zinc <br />Sample ID: <br />Iron <br />Zinc <br />Sample ID: <br />Iron <br />Zinc <br />LCS3 -35564 <br />C12101118 -001 BMS3 <br />C12101118 -001 BMSD <br />Method: E200.7 <br />Sample ID: MB- 121116A <br />Calcium <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.efiergleb.com <br />,Yna/dsai Etaileser Skye 1952 <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLImit Qual <br />7 Initial Calibration Verification Standard <br />1.04 <br />51.0 <br />5.07 <br />48.6 <br />47.4 <br />51.9 <br />1.03 <br />0.148 <br />506 <br />188 <br />500 <br />- 0.000200 <br />0.0668 <br />- 0.00830 <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />7 Interference Check Sample A <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />7 Interference Check Sample AB <br />0.133 mg /L <br />496 mg /L <br />188 mg /L <br />507 mg /L <br />0.000300 mg /L <br />0.0534 mg /L <br />1.03 mg /L <br />2 Method Blank <br />ND mg /L <br />0.002 mg /L <br />2 Sample Matrix Spike <br />2.58 mg /L <br />0.514 mg /L <br />2 Sample Matrix Spike Duplicate <br />2.58 mg /L <br />0.523 mg /L <br />2 Laboratory Control Sample <br />2.60 mg /L <br />0.515 mg /L <br />5 Method Blank <br />ND mg /L <br />Helena, MT 877 -472 -0711 • Billings, MT 800 - 735.4489 • Casper, WY 888 -235 -0515 <br />Gillette, WY 866486 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888- 890 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />0.10 <br />0.50 <br />0.030 <br />0.50 <br />0.50 <br />0.50 <br />0.010 <br />0.10 <br />0.50 <br />0.030 <br />0.50 <br />0.50 <br />0.50 <br />0.010 <br />0.10 <br />0.50 99 80 <br />0.030 94 80 <br />0.50 101 80 <br />0.50 <br />0.50 <br />0.010 103 80 <br />0.005 <br />0.002 <br />0.06 <br />104 <br />102 <br />101 <br />97 <br />95 <br />104 <br />103 <br />101 <br />94 <br />100 <br />95 <br />95 <br />95 <br />95 <br />95 <br />95 <br />95 <br />80 <br />80 <br />80 <br />Report Date: 12/18/12 <br />Work Order: C12101105 <br />105 <br />105 <br />105 <br />105 <br />105 <br />105 <br />105 <br />120 <br />120 <br />120 <br />120 <br />120 <br />120 <br />120 <br />Run: ICP2-C_121116A <br />Run: ICP2- C_121116A <br />0.030 104 85 115 <br />0.010 103 85 115 <br />Run: ICP2-C_121116A <br />0.030 103 70 130 <br />0.010 101 70 130 <br />Run: ICP2-C_121116A <br />0.030 103 70 130 <br />0.010 103 70 130 <br />Run: ICP2-C_121116A <br />ND - Not detected at the reporting limit. <br />Analytical Run: ICP2- C_121116A <br />11/16/12 12:28 <br />11/16/12 12:57 <br />11/16/12 13:01 <br />Batch: 35564 <br />11/16/12 21:40 <br />11/16/12 21:44 <br />11/16/12 21:56 <br />11/16/12 22:01 <br />0.1 20 <br />1.7 20 <br />Batch: R167330 <br />11/16/12 13:25 <br />Page 7 of 20 <br />