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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487(800) 334 -5493 <br />Rio Grande Silver, Inc. <br />Project ID: S12064 <br />Sample ID: WRSF -F <br />Wet Chemistry <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />Alkalinity (1312 DI) <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Chloride (1312 DI) <br />Fluoride (1312 DI) <br />Nitrate (1312 DI) <br />Nitrate /Nitrite as N <br />(1312 -DI) <br />Nitrite as N (1312 -DI) <br />Nitrogen, ammonia <br />(1312 -DI) <br />Phosphorus, ortho <br />dissolved (1312 -DI) <br />Sulfate (1312 DI) <br />SM2320B - Titration <br />SM4500CI -E <br />SM4500F -C <br />Calculation: NO3NO2 minus NO2 0 02 <br />M353.2 - Automated Cadmium 0 03 <br />Reduction <br />M353 2 - Automated Cadmium 0.01 BH <br />Reduction <br />M350 1 - Automated Phenate 0 07 B <br />M365.1 - Automated Ascorbic <br />Acid <br />D516 -02 - Turbidimetric <br />4 <br />4 <br />0 02 BH <br />15 <br />B <br />U <br />U <br />B <br />U <br />U <br />BH <br />BH <br />* mg /L <br />* mg /L <br />* mg /L <br />* mg /L <br />* mg /L <br />mg /L <br />* mg /L <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />Inorganic Analytical <br />Results <br />L97087 -06 <br />09/28/12 13:56 <br />10/02/12 <br />Soil <br />mg /L 2 20 10/15/12 0:00 abm <br />2 20 10/15/12 0 00 abm <br />2 20 10/15/12 0:00 abm <br />2 20 10/15/12 0:00 abm <br />1 5 10/16/12 9:48 Ihb <br />0.1 0 5 10/15/12 12:39 abm <br />0.02 0.1 10/22/12 11 40 calc <br />0 02 0 1 10/12/12 23:22 pjb <br />mg /L 0 01 0 05 10/18/12 23 55 pjb <br />mg /L 0 05 0 5 10/18/12 13:29 tcd <br />mg /L 0.01 0 05 10/12/12 22:31 pjb <br />mg /L 1 5 10/17/12 15:53 Ihb <br />REP IN 02 06 05 01 * Please refer to Qualifier Reports for details <br />Page 20 of 57 <br />