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ENERGY <br />LABORATORIES <br />Qualifiers: <br />www.energylab.com <br />Analytical &Waco Since 1952 <br />Method: E300.0 <br />Sample ID: ICB- 100112 -11 2 Method Blank <br />Chloride ND mg /L <br />Sulfate ND mg /L <br />Helena, MT 677 - 472 - 0711 • Billings, MT 800 735 - 4489 • Casper, WY 888 235 - 0515 <br />Gillette, WY 866 686 - 7175 • Rapid City, SD 886 - 672 - 1225 • College Station, TX 888 - 690 - 2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation Report Date: 10/23/12 <br />Project: Schwartz GW 9/27/2012 S26570 Work Order: C12100013 11 <br />Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E300.0 <br />Sample ID: ICV- 100112 -10 2 Initial Calibration Verification Standard <br />Chloride 9.96 mg /L 1.0 100 90 110 <br />Sulfate 40.2 mg /L 1.0 100 90 110 <br />0.04 <br />0.1 <br />Run: IC1-C 121001A <br />Analytical Run: IC1- C_121001 A <br />10/01/12 17:30 <br />Batch: R165252 <br />10/01/12 17:47 <br />Sample ID: LFB- 100112 -12 2 Laboratory Fortified Blank Run: IC1- C_121001A 10/01/12 18:05 <br />Chloride 9.89 mg /L 1.0 99 90 110 <br />Sulfate 40.2 mg /L 1.0 101 90 110 <br />Sample ID: 012100013- 001BMS 2 Sample Matrix Spike Run: IC1- C_121001A 10/01/12 18:40 <br />Chloride 70.7 mg /L 1.0 99 90 110 <br />Sulfate 1140 mg /L 4.2 90 110 A <br />Sample ID: 012100013- 001BMSD 2 Sample Matrix Spike Duplicate Run: IC1- C_121001A 10/01/12 18:57 <br />Chloride 70.1 mg /L 1.0 98 90 110 0.9 10 <br />Sulfate 1120 mg /L 4.2 90 110 1.7 10 A <br />RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In <br />accordance with the method % recovery is not calculated. <br />ND - Not detected at the reporting limit. MDC - Minimum detectable concentration <br />Page 13 of 20 <br />