2012-12-17_HYDROLOGY - M1977300 (3)

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ENERGY LABORATORIES Client: Cotter Corporation Project: Schwartz GW 9/26/2012 S26569 Method: E200.8 Sample ID: LRB 11 Method Blank Aluminum ND mg /L 0.0002 Antimony ND mg /L 0.0001 Calcium ND mg /L 0.007 Copper ND mg /L 3E -05 Iron ND mg /L 0.0006 Manganese ND mg /L 3E -05 Molybdenum ND mg /L 3E -05 Potassium 0.008 mg /L 0.004 Thallium ND mg /L 6E -05 Uranium ND mg /L 9E -06 Zinc ND mg /L 0.0002 Sample ID: LFB 11 Laboratory Fortified Blank Run: ICPMS4- C_121008A Aluminum 0.0554 mg /L 0.0010 111 85 115 Antimony 0.0510 mg /L 0.0010 102 85 115 Calcium 12.7 mg /L 0.0066 102 85 115 Copper 0.0554 mg /L 0.0010 111 85 115 Iron 1.31 mg /L 0.0010 105 85 115 Manganese 0.0525 mg /L 0.0010 105 85 115 Molybdenum 0.0525 mg /L 0.0010 105 85 115 Potassium 12.8 mg /L 0.0041 102 85 115 Thallium 0.0519 mg /L 0.0010 104 85 115 Uranium 0.0514 mg /L 0.00030 103 85 115 Zinc 0.0570 mg /L 0.0010 114 85 115 Sample ID: 012100115- 001BMS4 11 Sample Matrix Spike Run: ICPMS4- C_121008A Aluminum 0.0509 mg /L 0.030 102 70 130 Antimony 0.0537 mg /L 0.0010 107 70 130 Calcium 168 mg /L 1.0 70 130 Copper 0.0472 mg /L 0.0050 94 70 130 Iron 7.73 mg /L 0.030 70 130 Qualifiers: www.energylab.com Helena, MT 877 472 - 0711 • Billings, MT 800 - 135 - 4489 • Casper, WY 888 235 - 0515 AuktIcal &Waco Sliwa 1952 J Gillette, WY 866- 686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888- 690 -2218 QA/QC Summary Report Prepared by Casper, WY Branch Run: ICPMS4 C_121008A Revised Date: 10/26/12 Report Date: 10/22/12 Work Order: C12091083 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E200.8 Analytical Run: ICPMS4- C_121008A Sample ID: ICV 11 Initial Calibration Verification Standard 10/08/12 12:08 Aluminum 0.0498 mg /L 0.0010 100 90 110 Antimony 0.0548 mg /L 0.0010 110 90 110 Calcium 9.71 mg /L 0.0066 97 90 110 Copper 0.0513 mg /L 0.0010 103 90 110 Iron 1.00 mg /L 0.0010 101 90 110 Manganese 0.0494 mg /L 0.0010 99 90 110 Molybdenum 0.0506 mg /L 0.0010 101 90 110 Potassium 9.72 mg /L 0.0041 97 90 110 Thallium 0.0498 mg /L 0.0010 100 90 110 Uranium 0.0494 mg /L 0.00030 99 90 110 Zinc 0.0507 mg /L 0.0010 101 90 110 Batch: R165531 10/08/12 12:59 10/08/12 13:03 10/09/12 05:10 A A RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. ND - Not detected at the reporting limit. MDC - Minimum detectable concentration Page 11 of 21