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ENERGY <br />LABORATORIES <br />Project: Schwartz GW 9/20/2012 S26607 & S26608 Work Order: 012090782 <br />Client: Cotter Corporation <br />Analyte <br />Method: E300.0 <br />Sample ID: ICV- 092412 -10 2 Initial Calibration Verification Standard <br />Chloride 9.74 mg /L 1.0 97 90 110 <br />Sulfate 40.3 mg /L 1.0 101 90 110 <br />Method: E300.0 <br />Sample ID: ICB- 092412 -11 2 Method Blank <br />Chloride ND mg /L <br />Sulfate ND mg /L <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energylab.com Helena, MT 871- 472 -0711 • Billings, MT 800- 735 -4489 • Casper, WY 888 235 - 0515 <br />Analytical Excellence Sines 1952 i Gillette, WY 866 - 686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888- 690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />0.03 <br />0.10 <br />Run: IC2 -C 120924B <br />ND - Not detected at the reporting limit. <br />Report Date: 10/18/12 <br />Analytical Run: IC2- C_120924B <br />09/24/12 17:03 <br />Batch: R165020 <br />09/24/12 17:21 <br />Sample ID: LFB- 092412 -13 2 Laboratory Fortified Blank Run: IC2- C_120924B 09/24/12 17:56 <br />Chloride 9.65 mg /L 1.0 97 90 110 <br />Sulfate 39.8 mg /L 1.0 100 90 110 <br />Sample ID: LFBD- 092412 -14 2 Laboratory Fortified Blank Duplicate Run: IC2- C_120924B 09/24/12 18:13 <br />Chloride 9.64 mg /L 1.0 96 90 110 <br />Sulfate 39.7 mg /L 1.0 99 90 110 <br />Sample ID: C12090779- 001AMS 2 Sample Matrix Spike Run: IC2- C_120924B 09/24/12 19:40 <br />Chloride 11.1 mg /L 1.0 99 90 110 <br />Sulfate 51.9 mg /L 1.0 101 90 110 <br />Sample ID: C12090779- 001AMSD 2 Sample Matrix Spike Duplicate Run: IC2- C_120924B 09/24/12 19:58 <br />Chloride 11.3 mg /L 1.0 100 90 110 1.0 10 <br />Sulfate 52.6 mg /L 1.0 103 90 110 1.3 10 <br />Page 14 of 21 <br />