2012-12-17_HYDROLOGY - M1977300 (3)

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ENERGY LABORATORIES www.energylab.com Helena, MT 877 472 - 0711 • Billings, MT 800 - 735 - 4489 • Casper, WY 888 235 - 0515 Analytical Excellence Since 1952 I Gillette, WY 866- 686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888 - 690 -2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Cotter Corporation Report Date: 10/18/12 Project: Schwartz GW 9/13/12 S26638 Work Order: C12090499 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qua! Method: E200.7 Sample ID: C12090499- 001CMS2 7 Sample Matrix Spike Run: ICP2- C_121016A Calcium 405 mg /L 1.0 84 70 130 Copper 2.01 mg /L 0.0050 98 70 130 Manganese 3.41 mg /L 0.0010 96 70 130 Molybdenum 2.03 mg /L 0.0072 85 70 130 Potassium 101 mg /L 1.0 82 70 130 Sodium 235 mg /L 1.0 98 70 130 Zinc 2.00 mg /L 0.010 96 70 130 Sample ID: C12090499- 001CMSD 7 Sample Matrix Spike Duplicate Run: ICP2- C_121016A 10/16/12 15:31 Calcium 407 mg /L 1.0 86 70 130 0.6 20 Copper 2.01 mg /L 0.0050 98 70 130 0.2 20 Manganese 3.45 mg /L 0.0010 97 70 130 1.1 20 Molybdenum 2.07 mg /L 0.0072 87 70 130 1.9 20 Potassium 104 mg /L 1.0 86 70 130 3.3 20 Sodium 237 mg /L 1.0 101 70 130 1.1 20 Zinc 2.02 mg /L 0.010 97 70 130 0.7 20 Method: E200.7 Sample ID: ICV 2 Initial Calibration Verification Standard Boron 1.01 mg /L 0.10 101 95 105 Iron 4.88 mg /L 0.030 98 95 105 Sample ID: ICSA 2 Interference Check Sample A Boron - 0.00155 mg /L 0.10 Iron 170 mg /L 0.030 85 80 120 Sample ID: ICSAB 2 Interference Check Sample AB Boron 0.000540 mg /L 0.10 Iron 171 mg /L 0.030 86 80 120 Method: E200.7 Sample ID: MB -35047 2 Method Blank Boron ND mg /L Iron ND mg /L Qualifiers: RL - Analyte reporting limit. MDC - Minimum detectable concentration 0.003 0.004 Run: ICP4- C_121011 A Sample ID: LCS3 -35047 2 Laboratory Control Sample Run: ICP4- C_121011A Boron 0.543 mg /L 0.050 109 85 115 Iron 2.65 mg /L 0.030 106 85 115 Sample ID: C12090499- 001DMS3 2 Sample Matrix Spike Run: ICP4- C_121011A Boron 0.743 mg /L 0.050 98 70 130 Iron 2.51 mg /L 0.030 100 70 130 ND - Not detected at the reporting limit. Batch: R165910 10/16/12 15:27 Analytical Run: ICP4- C_121011A 10/11/12 15:15 10/11/12 15:29 10/11/12 15:33 Batch: 35047 10/11/12 19:44 10/11/12 19:47 10/11/12 19:59 Sample ID: C12090499- 001DMSD 2 Sample Matrix Spike Duplicate Run: ICP4- C_121011A 10/11/12 20:03 Boron 0.766 mg /L 0.050 102 70 130 3.0 20 Iron 2.55 mg /L 0.030 102 70 130 1.5 20 Page 10 of 23