2012-12-17_HYDROLOGY - M1977300 (2)

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ENERGY LA HOR R IES Client: Cotter Corporation Analyte Sample ID: LFB- 120827A Manganese Potassium Sodium Qualifiers: www.energylab.com Analytical Excellence Since 1851 Helena, MT 871- 472 -0711 • Billings, MT 800- 735 -4489 • Casper, WY 888- 235 -0515 Gillette, WY 866 - 686 - 7175 • Rapid City, SD 888 612 - 1225 • College Station, TX 888 - 690 - 221 B QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 09/11/12 Project: Schwartz GW 8/3/2012 S26545 Work Order: C12080184 Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E200.7 Sample ID: C12080184- 001EMS2 6 Sample Matrix Spike Run: ICP4- C_120823A Zinc 0.929 mg /L 0.010 86 70 130 Sample ID: C12080184- 001EMSD 6 Sample Matrix Spike Duplicate Run: ICP4- C_120823A 08/23/12 16:59 Aluminum 1.03 mg /L 0.030 100 70 130 14 20 Calcium 128 mg /L 1.0 96 70 130 8.0 20 Iron 1.03 mg /L 0.030 99 70 130 11 20 Magnesium 76.1 mg /L 1.0 102 70 130 9.0 20 Molybdenum 1.01 mg /L 0.0029 97 70 130 7.3 20 Zinc 0.966 mg /L 0.010 90 70 130 3.9 20 Method: E200.7 Sample ID: ICV 3 Initial Calibration Verification Standard Manganese 4.80 mg /L 0.010 96 95 105 Potassium 49.4 mg /L 0.50 99 95 105 Sodium 50.3 mg /L 0.50 101 95 105 Sample ID: ICSA 3 Interference Check Sample A Manganese - 0.00870 mg /L 0.010 Potassium - 0.0130 mg /L 0.50 Sodium 0.315 mg /L 0.50 Sample ID: ICSAB 3 Interference Check Sample AB Manganese 0.432 mg /L 0.010 86 80 120 Potassium - 0.0153 mg /L 0.50 Sodium 0.161 mg /L 0.50 Method: E200.7 Sample ID: MB- 120827A 3 Method Blank Manganese ND mg /L 0.0010 Potassium ND mg /L 0.04 Sodium ND mg /L 0.2 3 Laboratory Fortified Blank 0.927 mg /L 48.0 mg /L 48.1 mg /L Run: ICP4 -C 120827A Run: ICP4-C_120827A 0.010 93 85 115 0.50 96 85 115 0.50 96 85 115 Batch: R163707 08/23/12 16:56 Analytical Run. ICP4- C_120827A 08/27/12 14:44 08/27/12 14:59 08/27/12 15:03 Batch: R163828 08/27/12 15:07 08/27/12 15:10 Sample ID: C12080825 -001 BMS2 3 Sample Matrix Spike Run: ICP4- C_120827A 08/27/12 17:02 Manganese 0.970 mg /L 0.0010 94 70 130 Potassium 53.1 mg /L 1.0 102 70 130 Sodium 261 mg /L 1.0 70 130 A Sample ID: C12080825 -001 BMSD 3 Sample Matrix Spike Duplicate Run: ICP4- C_120827A 08/27/12 17:06 Manganese 0.964 mg /L 0.0010 93 70 130 0.6 20 Potassium 53.8 mg /L 1.0 104 70 130 1.2 20 Sodium 263 mg /L 1.0 70 130 0.6 20 A RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. ND - Not detected at the reporting limit. MDC - Minimum detectable concentration Page 8 of 19