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ENERGY <br />LA©ORATORIE i <br />Client: Cotter Corporation <br />Project: Schwartz GW 7/20/12 S26541 Work Order: C12070761 <br />Analyte <br />Method: E300.0 <br />Sample ID: ICV- 072312 -10 2 Initial Calibration Verification Standard <br />Chloride 10.3 mg /L 1.0 103 90 110 <br />Sulfate 40.6 mg /L 1.0 102 90 110 <br />Sample ID: ICBD- 072312 -12 2 Initial Calibration Blank, Instrument Blank <br />Chloride 0.0210 mg /L 1.0 0 <br />Sulfate 0 0830 mg /L 1 0 0 <br />Method: E300.0 <br />Sample ID: ICB- 072312 -11 2 Method Blank <br />Chloride ND mg /L <br />Sulfate ND mg /L <br />Sample ID: LFB- 072312 -13 <br />Chloride <br />Sulfate <br />Sample ID: C12070747- 001AMS <br />Chloride <br />Sulfate <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energylab.com I Helena, MT 877- 472 -0111 • Billings, MT 800 -735 -4489 • Casper, WY 888- 235 -0515 AnsryNCilExcellenceSince 1952 Gillette, WY 866- 686 -1175 • Rapid City, SD 888- 672 -1225 • College Station, TX 888 -690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />2 Laboratory Fortified Blank <br />10.0 mg /L <br />40.6 mg /L <br />2 Sample Matrix Spike <br />13.7 mg /L <br />54.6 mg /L <br />0.04 <br />0.1 <br />Run: IC1-C_120723A <br />0 <br />0 <br />Run: IC1-C_120723A <br />1.0 100 90 110 <br />1.0 101 90 110 <br />Run:IC1- C_120723A <br />1.0 103 90 110 <br />1.0 105 90 110 <br />ND - Not detected at the reporting limit. <br />Report Date: 08/17/12 <br />Analytical Run: IC1- C_120723A <br />07/23/12 18:10 <br />07/23/12 18:45 <br />Batch: R162333 <br />07/23/12 18:27 <br />07/23/12 19:02 <br />Sample ID: LFBD- 072312 -14 2 Laboratory Fortified Blank Duplicate Run: IC1- C_120723A 07/23/12 19'20 <br />Chloride 10.2 mg /L 1.0 102 90 110 1.9 10 <br />Sulfate 43.1 mg /L 1.0 108 90 110 5.9 10 <br />Sample ID: C12070747- 001AMSD 2 Sample Matrix Spike Duplicate Run: IC1- C_120723A 07/25/12 01:13 <br />Chloride 13.8 mg /L 1.0 104 90 110 0.7 10 <br />Sulfate 55.1 mg /L 1.0 106 90 110 0.9 10 <br />Page 10 of 18 <br />07/25/12 00:55 <br />