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ENERGY <br />L. AHOPATORIF <br />Method: E353.2 <br />Sample ID: MBLK <br />Nitrogen, Nitrate +Nitrite as N <br />AnelyrlcaIFxcellence Since 1952 <br />vow .energylab.com <br />Client: Cotter Corporation <br />Project: Schwartz GW 9/19/12 S26642 <br />Sample ID: LFB Laboratory Fortified Blank <br />Nitrogen, Nitrate +Nitrite as N 1.04 mg /L <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />Method Blank <br />ND mg /L 0.003 <br />Sample ID: B12091961 -001CMS Sample Matrix Spike <br />Nitrogen, Nitrate +Nitrite as N 1.10 mg /L <br />Sample ID: B12091961 -001CMSD Sample Matrix Spike Duplicate <br />Nitrogen, Nitrate +Nitrite as N 1.09 mg /L <br />Helena, MT 877- 472 -0711 • Billings, MT 800- 135 -4489 • Casper, WY 888- 235 -0515 <br />Gillette, WY 866 -686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888 - 690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Revised Date: 10/26/12 <br />Report Date: 10/17/12 <br />Work Order: C12090732 <br />Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E353.2 Analytical Run: SUB- B192516 <br />Sample ID: ICV Initial Calibration Verification Standard 09/28/12 07:55 <br />Nitrogen, Nitrate +Nitrite as N 22.8 mg /L 0.060 105 90 110 <br />Run: SUB- B192516 <br />Run: SUB- B192516 09/28/12 07:58 <br />0.010 106 90 110 <br />Run: SUB- B192516 09/28/12 10:56 <br />0.010 103 90 110 <br />Run: SUB- B192516 09/28/12 10:57 <br />0.010 102 90 110 0.2 10 <br />ND - Not detected at the reporting limit. <br />Batch: B_R192516 <br />09/28/12 07:56 <br />Page 14 of 21 <br />