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ENERGY <br />L.ABORATORIL S <br />wyw.energylab.com <br />Analytical Excellence Since 1952 <br />Client: Cotter Corporation <br />Project: Schwartz GW 8/31/2012 S26629 <br />Method: E200.8 <br />Sample ID: LRB 5 Method Blank <br />Antimony 0.0004 mg /L 0.0001 <br />Copper ND mg /L 3E -05 <br />Thallium ND mg /L 6E -05 <br />Uranium 0.0002 mg /L 9E -06 <br />Zinc ND mg /L 0.0002 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />Helena, MT 877 -472 -0111 • Billings, MT 800- 735 -4489 • Casper, WY 888 -235 -0515 <br />Gillette, WY 866 -686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888 - 690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.8 Batch: 34925 <br />Sample ID: C12090028 -001BMSD 8 Sample Matrix Spike Duplicate Run: ICPMS4- C_120910A 09/11/12 05:12 <br />Lead 0.498 mg /L 0.0010 100 70 130 1.4 20 <br />Manganese 2.51 mg /L 0.0010 99 70 130 0.2 20 <br />Thallium 0.503 mg /L 0.00050 101 70 130 0.9 20 <br />Zinc 0.515 mg /L 0.010 101 70 130 0.1 20 <br />Method: E200.8 Analytical Run: ICPMS4- C_120925A <br />Sample ID: ICV 5 Initial Calibration Verification Standard 09/25/12 12:46 <br />Antimony 0.0540 mg /L 0.0010 108 90 110 <br />Copper 0.0477 mg /L 0.0010 95 90 110 <br />Thallium 0.0505 mg /L 0.0010 101 90 110 <br />Uranium 0.0495 mg /L 0.00030 99 90 110 <br />Zinc 0.0500 mg /L 0.0010 100 90 110 <br />Run' ICPMS4- C_120925A <br />Sample ID: LFB 5 Laboratory Fortified Blank Run: ICPMS4- C_120925A <br />Antimony 0.0469 mg /L 0.0010 93 85 115 <br />Copper 0.0512 mg /L 0.0010 102 85 115 <br />Thallium 0.0514 mg /L 0.0010 103 85 115 <br />Uranium 0.0506 mg /L 0.00030 101 85 115 <br />Zinc 0.0524 mg /L 0.0010 105 85 115 <br />Sample ID: 012090381- 004BMS4 5 Sample Matrix Spike Run: ICPMS4- C_120925A <br />Antimony 0.0506 mg /L 0.0010 101 70 130 <br />Copper 0.0448 mg /L 0.0050 89 70 130 <br />Thallium 0.0525 mg /L 0.00050 105 70 130 <br />Uranium 0.0626 mg /L 0.00030 105 70 130 <br />Zinc 0.0770 mg /L 0.010 101 70 130 <br />Revised Date: 11/01/12 <br />Report Date: 10/05/12 <br />Work Order: C12090026 <br />Batch: R165055 <br />09/25/12 13:21 <br />09/25/12 13:25 <br />09/25/12 17:11 <br />Sample ID: C12090381- 004BMSD 5 Sample Matrix Spike Duplicate Run: ICPMS4- C_120925A 09/25/12 17:15 <br />Antimony 0.0512 mg /L 0.0010 102 70 130 1.1 20 <br />Copper 0.0460 mg /L 0.0050 92 70 130 2.5 20 <br />Thallium 0.0523 mg /L 0.00050 105 70 130 0.3 20 <br />Uranium 0.0632 mg /L 0.00030 106 70 130 0.8 20 <br />Zinc 0.0790 mg /L 0.010 105 70 130 2.6 20 <br />ND - Not detected at the reporting limit. <br />Page 11 of 20 <br />