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ENERGY <br />Ay(]11AI Of.fl 5 <br />Project: Schwartz -SW 9/05/12 S26562 Work Order: C12090140 <br />Client: Cotter Corporation <br />Analyte <br />Method: E300.0 Analytical Run: IC1- C_120906A <br />Sample ID: ICV- 090612 -10 Initial Calibration Verification Standard 09/06/12 16:04 <br />Chloride 9.64 mg /L 1.0 96 90 110 <br />Method: E300.0 Batch: R164323 <br />Sample ID: ICB- 090612 -111 Method Blank Run: IC1- C_120906A 09/06/12 16:21 <br />Chloride ND mg /L 0.04 <br />Sample ID: LFB- 090612 -12 Laboratory Fortified Blank Run: IC1- C_120906A 09/06/12 16:38 <br />Chloride 9.90 mg /L 1.0 99 90 110 <br />Sample ID: C12090191- 001AMS Sample Matrix Spike Run: IC1- C_120906A 09/07/12 18:10 <br />Chloride 13.2 mg /L 1.0 102 90 110 <br />Sample ID: C12090191- 001AMSD Sample Matrix Spike Duplicate Run: IC1- C_120906A 09/07/12 18:28 <br />Chloride 13.4 mg /L 1.0 104 90 110 1.2 10 <br />Method: E300.0 Analytical Run: IC1- C_120910A <br />Sample ID: ICV- 091012 -10 Initial Calibration Verification Standard 09/10/12 19:43 <br />Sulfate 39.0 mg /L 1.0 97 90 110 <br />Method: E300.0 Batch: R164376 <br />Sample ID: ICB- 091012 -11 Method Blank Run: IC1- C_120910A 09/10/12 20:00 <br />Sulfate ND mg /L 0.1 <br />Sample ID: LFB- 091012 -12 Laboratory Fortified Blank Run IC1- C_120910A 09/10/12 20:18 <br />Sulfate 39.7 mg /L 1.0 99 90 110 <br />Sample ID: C12090211- 001AMS Sample Matrix Spike Run: IC1- C_120910A 09/10/12 20:52 <br />Sulfate 165 mg /L 1.7 101 90 110 <br />Sample ID: C12090211- 001AMSD Sample Matrix Spike Duplicate Run IC1- C_12091OA 09/10/12 21:10 <br />Sulfate 168 mg /L 1.7 105 90 110 1.7 10 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energylab.com ( Helena, MT 877 472 - 0711 • Billings, MT 800 735 - 4489 • Casper, WY 888 235 - 0515 <br />A° * a Eminence nc• Sh ce 1952 ) Gillette, WY 866 - 686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888- 690 -2218 <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />ND - Not detected at the reporting limit. <br />Report Date: 10/02/12 <br />Page 20 of 28 <br />