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ENERGY <br />LAH 01-if 1 (;Hi -;� <br />Client: Cotter Corporation <br />Analyte <br />Qualifiers: <br />RL - Analyte reporting limit <br />MDC - Minimum detectable concentration <br />www.energylab.com Helena, MT 877 472 - 0711 • Billings, MT 800 735 - 4489 • Casper, WY 888 - 235 - 0515 <br />AsslytIcal &" • Axe 1052 Gillette, WY 866- 686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888 -690 -2218 <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch <br />Report Date: 10/02/12 <br />Project: Schwartz -SW 9/05/12 S26562 Work Order: C12090140 <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.7 Analytical Run: ICP2- C_120912A <br />Sample ID: ICV 6 Initial Calibration Verification Standard 09/12/12 11:12 <br />Aluminum 4.85 mg /L 0.10 97 95 105 <br />Boron 1.03 mg /L 0.10 103 95 105 <br />Iron 5.14 mg /L 0.030 103 95 105 <br />Manganese 4.98 mg /L 0.010 100 95 105 <br />Molybdenum 0.982 mg /L 010 98 95 105 <br />Zinc 1.02 mg /L 0.010 102 95 105 <br />Sample ID: ICSA 6 Interference Check Sample A 09/12/12 11:59 <br />Aluminum 495 mg /L 010 99 80 120 <br />Boron - 0.0192 mg /L 0.10 <br />Iron 192 mg /L 0.030 96 80 120 <br />Manganese - 0.00270 mg /L 0.010 <br />Molybdenum - 0.0132 mg /L 0.10 <br />Zinc - 0.0102 mg /L 0.010 <br />Sample ID: ICSAB 6 Interference Check Sample AB <br />Aluminum 496 mg /L 0.10 99 80 120 <br />Boron - 0.0255 mg /L 0.10 <br />Iron 191 mg /L 0.030 95 80 120 <br />Manganese 0.495 mg /L 0.010 99 80 120 <br />Molybdenum - 0.0148 mg /L 0.10 <br />Zinc 1.01 mg /L 0.010 101 80 120 <br />Method: E200.7 <br />Sample ID: MB -34945 6 Method Blank <br />Aluminum ND mg /L 0.009 <br />Boron ND mg /L 0.01 <br />Iron ND mg /L 0.005 <br />Manganese ND mg /L 0.0002 <br />Molybdenum ND mg /L 0.002 <br />Zinc 0.002 mg /L 0.002 <br />Run ICP2- C_120912A <br />Sample ID: LCS3 -34945 6 Laboratory Control Sample Run: ICP2- C_120912A <br />Aluminum 2.38 mg /L 0.030 95 85 115 <br />Boron 0.470 mg /L 0.050 94 85 115 <br />Iron 2.46 mg /L 0.030 98 85 115 <br />Manganese 2.42 mg /L 0.0010 97 85 115 <br />Molybdenum 0.482 mg /L 0.0023 96 85 115 <br />Zinc 0 487 mg /L 0 010 97 85 115 <br />Sample ID: C12090140 -001 DMS3 6 Sample Matrix Spike Run: ICP2- C_120912A <br />Aluminum 2 37 mg /L 0.030 95 70 130 <br />Boron 0.674 mg /L 0.050 95 70 130 <br />Iron 2.49 mg /L 0.030 98 70 130 <br />Manganese 2.79 mg /L 0.0010 98 70 130 <br />Molybdenum 0.721 mg /L 0 0023 97 70 130 <br />Zinc 0.499 mg /L 0 010 97 70 130 <br />ND - Not detected at the reporting limit. <br />Page 10 of 28 <br />09/12/12 12:03 <br />Batch: 34945 <br />09/12/12 13:48 <br />09/12/12 13:52 <br />09/12/12 14:04 <br />