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ACZ Laboratories, Inc. <br />r <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: AP -2 <br />Metals Analysis <br />Px# as o.o <br />ePA moi Hatt tl tat <br />03,t :A 3(a tacit *% Wel POL <br />OM* <br />Acuasi <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Mangan..., dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />epA ti 1 # - katt <br />i9ra8 Ott <br />3EiQ L.Inft% MtIL <br />t2L Oat* ,> mf y <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate/Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) ©180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />REPIN.02.06.05.01 <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 1CP <br />M200.7 ICP <br />M200.7 ICP <br />SM23208 - Titration <br />Calculation <br />M325.2 - Coloimetric <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />SM4500 SO4 -D <br />Calculation <br />Calculation <br />64.6 <br />0.12 <br />46.3 <br />0.599 <br />2.4 <br />66.8 <br />434 <br />434 <br />-1.9 <br />10.5 <br />10.1 <br />12 <br />352 <br />Calculation: NO3NO2 minus NO2 0.03 <br />M353.2 - Automated Cadmium 0.03 <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />M160.1 - Gravimetric 510 <br />USGS - 11738 -78 1.S7 <br />70 <br />523 <br />0.98 <br />U <br />U <br />B <br />B <br />U <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />mg/L <br />mg/L <br />mgL <br />mgA <br />mg/ <br />02 <br />0.02 <br />0.2 <br />0.005 <br />0.3 <br />0.3 <br />1 <br />0.05 <br />1 <br />0.03 <br />1 <br />L59074-04 <br />09/26/0611:10 <br />09/26/06 <br />Ground Water <br />10/04/06 21:45 <br />10/04/06 21:45 <br />10/04/06 21:45 <br />10104/06 21:45 <br />10/04/06 21:45 <br />10/04/06 21:45 <br />mg/L 2 20 10/09/06 0:00 <br />m <br />mgL <br />mL <br />meq/L <br />meq <br />mg/L <br />mg/L <br />2 <br />2 <br />2 <br />0.1 <br />0.1 <br />1 <br />1 <br />20 <br />20 <br />20 <br />0.5 <br />0.5 <br />5 <br />7 <br />10/09/06 0:00 <br />10/09/06 0:00 <br />10/09/06 0:00 <br />10/23/06 0:00 <br />10/23/06 0:00 <br />10/23/06 0:00 <br />10/03/06 17:01 <br />10/23/06 0:00 <br />09/27/06 17:52 <br />09/28/06 17:38 <br />mg/L 0.02 0.1 10/23/06 0:00 <br />mg/L 0.02 0.1 09/27/06 22:19 <br />mg/L 0.01 0.05 09127/06 22:19 <br />mg/L 10 20 10/02/0616:03 <br />mg/L <br />mL <br />0.03 0.15 10/23/06 0:00 calc <br />10 50 10/17/0615:52 <br />10 50 10/23/06 0:00 <br />10/23/06 0:00 <br />calc <br />calk <br />catc <br />0 <br />calk <br />mis <br />ink <br />ct <br />alc <br />calk <br />• Please refer to Qualifier Reports for detail <br />I L59074: Page 5 of 11 I <br />wf9 <br />Wfg <br />wt9 <br />wt9 <br />g <br />wt9 <br />ct <br />ct <br />ct <br />c t <br />ct <br />