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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: <br />Field Data <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />Conductivity (Field) <br />pH (Field) <br />Temperature (Field) <br />Metals Analysis <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Manganese, dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) @180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />REPIN.02.06.05.01 <br />AP -2 <br />Field Measurement <br />Field Measurement <br />Field Measurement <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />SM2320B - Titration <br />Calculation <br />SM4500CI -E <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />SM2540C <br />USGS -11738-78 <br />SM4500 SO4 -D <br />Calculation <br />Calculation <br />600 <br />8.0 <br />14.0 <br />46.8 <br />0.09 <br />31.3 <br />0.505 <br />1.6 B <br />25.6 <br />22 <br />300 <br />-5.4 <br />6.8 <br />6.1 <br />7 <br />246 <br />350 <br />0.71 <br />U <br />0.04 B <br />0.04 B <br />U <br />30 B <br />332 <br />1.05 <br />mS /cm <br />units <br />* C <br />mg /L <br />mg/L <br />mg/L <br />mg/L <br />mg /L <br />mg/L <br />mg /L <br />mg /L <br />mg/L <br />meq /L <br />meq /L <br />mg /L <br />mg/L <br />mg/L <br />mg /L <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />Inorganic Analytical <br />Results <br />0.2 <br />0.02 <br />0.2 <br />0.005 <br />0.3 <br />0.3 <br />0.1 <br />0.1 <br />1 <br />1 <br />1 <br />0.05 <br />1 <br />0.03 <br />2 <br />2 <br />0.5 <br />0.5 <br />5 <br />7 <br />L70560 -02 <br />07117108 10:20 <br />07118108 <br />Ground Water <br />07/17/08 10:20 <br />07/17/08 10:20 <br />07/17/08 10:20 <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />07/26/08 16:32 <br />07/26/08 16:32 <br />07/26/08 16:32 <br />07/29/08 12:33 <br />07/29/08 12:33 <br />07/26/08 16:32 <br />Parameter <br />EPA Method <br />Result Qual XQ Untts MDL PQL <br />Date Analyst <br />279 mg/L 2 20 07/21/08 0:00 <br />2 20 07/21/08 0:00 <br />2 20 07/21/08 0:00 <br />2 20 07/21/08 0:00 <br />07/30/08 0:00 <br />07/30/08 0:00 <br />07/30/08 0:00 <br />07/21/08 16:03 <br />07/30/08 0:00 <br />07/18/08 12:34 <br />07/18/08 15:47 <br />mg/L 0.02 0.1 07/30/08 0:00 <br />mg/L 0.02 0.1 07/18/08 19:14 <br />mg/L 0.01 0.05 07/18/08 19:14 <br />mg/L 10 20 07/22/0814:14 <br />0.03 0.15 07/30/08 0:00 <br />10 50 07/21/08 10:26 <br />10 50 07/30/08 0:00 <br />07/30/08 0:00 <br />• Please refer to Qualifier Reports for details. <br />Page 4 of 11 <br />jc <br />k <br />jc <br />aeh <br />aeh <br />aeh <br />aeh <br />aeh <br />aeh <br />tbd <br />tbd <br />tbd <br />tbd <br />calc <br />calc <br />calc <br />Ibn <br />calc <br />gkj <br />tbd <br />calc <br />pjb <br />pjb <br />tbd <br />calc <br />gkj <br />calc <br />calc <br />