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ACZ <br />Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487(800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: <br />Field Data <br />Parameter <br />EPA Method <br />Result Qual Units MDL PQL Date Analyst <br />Conductivity (Field) <br />pH (Field) <br />Temperature (Field) <br />Metals Analysis <br />Parameter <br />EPA Method <br />Result Qual Units MDt <br />PQL Date Analyst <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Manganese, dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />Parameter <br />EPA Method <br />Result Qual Units MDL PQL <br />Date Analyst <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) @180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />REPIN.01.11.00.0 <br />AP -1 <br />Field Measurement <br />Field Measurement <br />Field Measurement <br />M200.7 ICP <br />M200 7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />SM2320B - Titration <br />Calculation <br />M325.2 - Colorimetric <br />SM23408 - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />M160.1 - Gravimetric <br />USGS -11738-78 <br />M375.3 - Gravimetric <br />Calculation <br />Calculation <br />300 <br />7.8 <br />12.0 <br />40.5 <br />0.12 <br />31.6 <br />0.435 <br />11 <br />20.3 <br />198 mg /L 2 10 06/21/02 0 hap <br />198 <br />10.0 <br />4.5 <br />5.5 <br />4 <br />231 <br />0.07 <br />0.07 <br />umhos /cm <br />units <br />C <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />U mg /L <br />U mg /L <br />mg /L <br />meq /L <br />meq /L <br />8 mg /L <br />mg /L <br />B <br />B <br />U <br />ACZ ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />mg /L <br />mg /L <br />Inorganic Analytical <br />Results <br />0.2 <br />0.01 <br />0.2 <br />0.005 <br />0.3 <br />0.3 <br />0.1 <br />0.1 <br />1 <br />1 <br />1 <br />0 05 <br />1 <br />0.03 <br />1 <br />1 <br />2 10 06/21/02 0:00 <br />2 10 06/21/02 0:00 <br />2 10 06/21/02 0:00 <br />0.5 <br />0.5 <br />5 <br />7 <br />L37320-01 <br />06/19102 11:50 <br />06/20/02 <br />Ground Water <br />06/19/02 13:50 <br />06/19/02 13:50 <br />06/19/02 13:50 <br />07/14/02 19:31 <br />07/14/02 19:31 <br />07/14/02 19:31 <br />07/18/02 6:37 <br />07/18/02 6:37 <br />07/18/02 6:37 <br />07/18/02 15:42 <br />07/18/02 15:42 <br />07/18/02 15:42 <br />06/26/02 14:52 <br />07/18/02 15:42 <br />06/20/02 11 <br />06/20/02 23:00 <br />jm <br />jm <br />jm <br />bf <br />bf <br />bf <br />kdw <br />kdw <br />kdw <br />hap <br />hap <br />hap <br />calc <br />calc <br />talc <br />clt <br />talc <br />hap <br />ey <br />0.02 0.1 07/18/02 15:42 calc <br />0 02 0.1 06/20/02 12:23 ksj <br />mg /L 0.01 0.05 06/20/02 12:23 ksj <br />270 mg /L 10 20 06/20/0213 <br />Isa <br />0.58 0 03 0.15 07/18/02 15 calc <br />20 <br />237 <br />1.14 <br />mg /L <br />mg /L <br />10 20 06/21/02 20:36 <br />10 50 07/18/02 15:42 <br />07/18/02 15:42 <br />ey <br />calc <br />talc <br />L37320: Page 2 of 7 <br />