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ACZ Laboratories, Inc. <br />2773 Downhill Dnve Steamboat Springs, CO 80487 (800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: <br />Field Data <br />Conductivity (Field) <br />pH (Field) <br />Temperature (Field) <br />Metals Analysis <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Manganese, dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) @180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />REPIN.02.06.05.01 <br />AP -1 <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL Date Analyst <br />Field Measurement <br />Field Measurement <br />Feld Measurement <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />M200.7 ICP <br />M200 7 ICP <br />M200 7 ICP <br />M200 7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />SM2320B - Titration <br />Calculation <br />SM4500CI -E <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />SM2540C <br />USGS -11738-78 <br />SM4500 SO4 -D <br />Calculation <br />Calculation <br />600 <br />7.8 <br />120 <br />45.1 <br />0.14 <br />36.2 <br />0 468 <br />0.7 B <br />18.3 <br />6 <br />315 <br />-6.3 <br />6.8 <br />6.0 <br />4 <br />262 <br />350 <br />0 49 <br />B <br />U <br />B <br />U <br />20 B <br />317 <br />1.10 <br />umhos /cm <br />units <br />C <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />meq/L <br />meq /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />0.1 <br />01 <br />1 <br />1 <br />inorganic Analytical <br />Results <br />0.2 <br />0.02 <br />0.2 <br />0.005 <br />0.3 <br />0.3 <br />1 <br />0.05 <br />1 <br />0 03 <br />2 <br />2 <br />0.5 <br />05 <br />5 <br />7 <br />L84991 -01 <br />10/20/10 12:05 <br />10/21/10 <br />Ground Water <br />10/20/10 12:05 <br />10/20/10 12:05 <br />10/20/10 12:05 <br />10/28/10 18:40 <br />10/28/10 18:40 <br />10/28/10 18:40 <br />10/28/10 18:40 <br />10/29/10 11:36 <br />10/29/10 11:36 <br />2 20 10/23/10 0:00 <br />2 20 10/23/10 0:00 <br />2 20 10/23/10 0:00 <br />11/02/10 11:18 <br />11/02/10 11:18 <br />11/02/10 11:18 <br />11/01/10 13:05 <br />11/02/10 11:18 <br />10/21/10 14:17 <br />10/21/10 14:30 <br />10 50 10/29/1011:00 <br />10 50 11/02/10 11:18 <br />11/02/10 11:18 <br />Page 2 of 10 <br />Im <br />im <br />Im <br />ear <br />ear <br />ear <br />ear • <br />ear <br />ear <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />309 mg /L 2 20 10/23/10 0:00 Ihb <br />Ihb <br />Ihb <br />Ihb <br />calc <br />calc <br />calc <br />itk <br />calc <br />abm <br />abm <br />0.16 mg /L 0 02 0 1 11/02/10 11:18 calc <br />0.16 mg /L 0.02 0.1 10/21/10 21:05 pjb <br />mg /L 0.01 0 05 10/21/10 21:05 pjb <br />mg /L 10 20 10/22/10 12:32 abm <br />0.03 0.15 11/02/10 11:18 calc <br />abm <br />calc <br />calc <br />• Please refer to Qualifier Reports for details. <br />