2012-09-28_REVISION - M1977307 (27)

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wwwenergylab.com Helena MT 877 - 472 -0711 • Billings, MT 800 -735 -4489 4, Casper WY 888 - 235 -0515 Analytical Excellence Since 1952 Gillette, WY 866- 686 -7175 • Rapid City, SD 888- 672 -1225 ^ College Statiar_ TX 888- 690 -2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: O'Connor Design Inc Project: CM -25 Analyte Method: SW6020 Sample ID: ICSAB Barium Beryllium Cadmium Chromium Copper Iron Lead Manganese Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc Method: SW6020 Sample ID: MB -33660 Aluminum Antimony Arsenic Barium Beryllium Cadmium Chromium Copper Iron Lead Manganese Molybdenum Nickel Selenium Silver Thallium Uranium Vanadium Zinc Sample ID: LCS3 -33660 Aluminum Antimony Arsenic Barium Qualifiers: 'L - Analyte reporting limit ND - Not detected at the reporting limit. ADC - Minimum detectable concentration Batch 33660 19 Method Blank Report Date: 06/18/12 Run ICPMS4- C_120517A 05/17/12 19 58 0.03 mg /L 0 001 Work Order: C12050462 Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual 0 008 mg /L 0 -0001 ND mg/L Analytical Run ICPMS4- C_120517A 19 Interference Check Sample AB 9E -05 mg1L 4E -05 05/17/12 12 42 2 75E -05 mg /L 00010 0 001 mg /L 6E -05 1 10E -05 mg /L 0 010 0.0002 mg /L 3E -05 00102 mg /L 00010 102 70 130 4E -05 00105 mg /L 00010 105 70 130 7E -05 mg /L 0.0110 mg /L 00010 110 70 130 1 05 mg /L 00010 105 70 130 174E -05 mg /L 0.0010 0 -008 mg /L 00005 00102 mg /L 00010 102 70 130 24 mg /L 00206 mg /L 00010 103 70 130 80 120 00108 mg /L 0.0010 108 70 130 100 610E -06 mg /L 0.0010 00104 mg /L 00010 104 70 130 1 88E -05 mg /L 00010 136E -05 mg /L 0.00030 3 70E -06 mg /L 00010 00112 mg /L 00010 112 70 130 Qualifiers: 'L - Analyte reporting limit ND - Not detected at the reporting limit. ADC - Minimum detectable concentration Batch 33660 19 Method Blank Run ICPMS4- C_120517A 05/17/12 19 58 0.03 mg /L 0 001 ND mg /L 5E -05 00008 mg /L 7E -05 0 008 mg /L 0 -0001 ND mg/L 6E -05 9E -05 mg1L 4E -05 0 002 mg /L 0.001 0 001 mg /L 6E -05 003 mg /L 0.0009 0.0002 mg /L 3E -05 0.0010 mg /L 00002 9E -05 mg /L 4E -05 0.0003 mg /L 6E -05 7E -05 mg /L 6E -05 00006 mg /L 2E -05 ND mg /L 5E -05 0.0003 mg /L 5E -05 0.01 mg /L 7E -05 0 -008 mg /L 00005 19 Laboratory Control Sample Run ICPMS4- C_120517A 05/17/12 20 03 24 mg /L 0.030 97 80 120 047 mg /L 00010 94 80 120 0.42 mg /L 00010 85 80 120 051 mg /L 0 050 100 80 120 Qualifiers: 'L - Analyte reporting limit ND - Not detected at the reporting limit. ADC - Minimum detectable concentration