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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Account: GRAYLING/The Mining Company <br />Bottle Order: B027973 <br />Sampling supplies <br />ACZ Coolers <br />1 1 <br />1 1 <br />1 1 <br />1 1 <br />I 1 <br />1 1 <br />1 <br />2 <br />1 <br />28 <br />Prepared By /Date: <br />COC <br />SEAL <br />RETURN <br />LABELS <br />PACK Qty ACZ 1D <br />Size Weight <br />UPS Tracking Number <br />3087 <br />2931 <br />Sample Quantity: 2 <br />F 2 ORANGE <br />ri 1 PURPLE <br />1 RAW <br />2 RED CUBE <br />1 RED PC <br />1 RED RAD <br />1 STERILE <br />1 TAN <br />1 WHITE <br />1 YELLOW <br />GLASS <br />Large 18 <br />Large 11 <br />Quote number: ORVIS- UMT -CDPS <br />Chain of Custody <br />Custody Seal <br />Retum Address <br />Sample Labels <br />PACK Qty Type <br />Size Filter/Raw /Preserve <br />InstruCt <br />1 GREEN PC 250 ML Green pre - cleaned <br />Filtered/Nitiric <br />1 GREEN PD PC 250 ML Green pre - cleaned <br />Raw /Nitric <br />1000 ML Raw/Hydrochloric <br />500 ML Raw /NaOH <br />500 ML Raw <br />4 L Raw /Nitnc <br />250 ML Red pre - cleaned <br />Raw /Nitric <br />1000 ML Raw /Nitric <br />100 ML Raw /Sodium <br />Thiosulfate <br />125 ML Raw /NaOH & Zinc <br />Acetate <br />250 ML Filtered <br />250 ML Raw /Sulfuric <br />Bill to Account: <br />Ship Date Requested: <br />Request Placed at: <br />Service Requested: <br />Chain of Custody, 1 for 10 samples. <br />Custody seals for cooler, two for each cooler. <br />Return Address label, one for each cooler. <br />ACZ supplied labels for sample containers <br />1 28101300300307798 <br />1Z8101300300307803 <br />Discharge Analysis <br />ACZ is responsible for necessary sample filtering <br />Bottle Ord : r <br />Packing <br />Bill to ACZ <br />07/12/2012 <br />07/11/2012 09:51 <br />UPS Ground <br />Metals (dissolved including ICPMS) - This is a Filtered samle <br />Completely fill container. <br />Metals (potentially dissolved including ICPIv1S) - Do not overfill as <br />there is Nitric Acid in the bottle. <br />Oil and Grease - Do not overfill as there is Hydrochloric Acic in the <br />bottle. <br />Cyanide - Do not overfill as there is Sodium Hydroxide it the bottle. <br />Wet Chemistry (analyses that do not require preservative; or <br />filtration) - Completely fill container. <br />Radiochemistry (total) - Do not overfill as there is Nitric Acid n the <br />bottle. <br />Metals (total including ICPMS) - Do not overfill as there is Nitric <br />Acid in the bottle. <br />Radiochemistry (total) - Do not overfill as there is Nitric Acid in the <br />bottle. <br />Coliforms - Completely fill container with sample Coliforms require <br />testing within 24 hours of sampling time. Please call ACZ If Fnor <br />arrangements have not been made so we are prepared for th <br />arrival of this sample. <br />Sulfide - Do not overfill as there is Sodium Hydroxide and Zur: <br />Acetate in the bottle. <br />Wet chemistry (dissolved) - This is a filiterec sample. Couple :ely <br />fill container. <br />COD, TOC. Phenols, and total wet chemistry analysis. Dc not <br />overfill as there is Sulfuric Acid in the bottle. <br />laa <br />Page 1 of 2 <br />Page 36 of 54 <br />