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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Western Fuels New Horizon Mine <br />Project ID: <br />Sample ID: <br />Wet Chemistry <br />NORTH COAL CANYON <br />Parameter <br />EPA Method <br />Result Quail XQ Units MDL PQL <br />Date Analyst <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Ammonia as N, un- <br />ionized <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Conductivity @25C <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Nitrogen, ammonia <br />pH (lab) <br />pH <br />pH measured at <br />Phosphate <br />Phosphorus, ortho <br />dissolved <br />Residue, Filterable <br />(TDS) @180C <br />Residue, Non - <br />Filterable (TSS) <br />@105C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate. <br />Sulfide as S <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />SM2320B - Titration <br />M350.1 - Calculation <br />Calculation <br />SM4500CI -E <br />SM2510B <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 2.09 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />M350.1 - Automated Phenate <br />SM4500H+ B <br />Calculation based on Ortho <br />Phosphorus <br />M365.1 - Automated Ascorbic <br />Acid <br />SM2540C <br />SM2540D <br />USGS - 11738 -78 <br />D516 -02 - Turbidimetric <br />376.2 - Methylene Blue <br />Calculation <br />Calculation <br />470 <br />18 <br />489 <br />7.6 <br />39.9 meq /L 0.1 0.5 <br />46.5 meq /L 0.1 0.5 <br />66 mg /L 1 5 <br />3030 umhos /cm 1 10 <br />1800 mg /L 1 7 <br />mg /L 0.02 0.1 03/21/11 11:59 calc <br />2.09 • mg /L 0.02 0.1 03/10/11 21:51 pjb <br />8.3 <br />21.0 <br />2650 <br />9 <br />2.48 <br />1340 <br />2480 <br />1.07 <br />B <br />U <br />U <br />H <br />H <br />HU <br />U • mg /L 0.05 <br />H <br />U <br />U <br />B <br />U <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />Inorganic Analytical <br />Results <br />mg /L 2 20 03/11/11 0:00 <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />units <br />C <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />2 <br />2 <br />2 <br />0.01 <br />mg /L 0.01 0.05 03/10/11 21:51 pjb <br />0.1 <br />0.1 <br />0.03 <br />50 <br />0.02 <br />10 <br />20 <br />20 <br />20 <br />0.05 <br />0.5 03/17/11 15:41 mpb <br />0.1 <br />0.1 <br />0.15 <br />mg /L 0.01 0.05 03/09/11 19:33 pjb <br />mg /L 10 20 03/10/11 17:34 las <br />mg /L 5 20 03/11/11 15:39 cra <br />0.03 0.15 03/21/11 11:59 calc <br />300 <br />0.1 <br />50 <br />L86882 -02 <br />03/08/11 09:08 <br />03/09/11 <br />Surface Water <br />03/11/11 0:00 <br />03/11/11 0:00 <br />03/11/11 0:00 <br />03/21/11 11:59 <br />03/21/11 11:59 <br />03/21/11 11:59 <br />03/21/11 11:59 <br />03/15/11 11:08 <br />03/11/11 22:58 <br />03/21/11 11:59 <br />03/09/11 14:16 <br />03/09/11 16:48 <br />03/11/11 0:00 <br />03/11/11 0:00 <br />03/21/11 11:59 <br />03/18/11 13:47 <br />03/09/11 10:21 <br />03/21/11 11:59 <br />03/21/11 11:59 <br />las <br />las <br />las <br />las <br />calc <br />calc <br />calc <br />calc <br />ccp <br />las <br />calc <br />cra <br />Ihb <br />las <br />las <br />calc <br />itk <br />las <br />calc <br />calc <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 5 of 15 <br />