2012-08-02_HYDROLOGY - M1977300 (2)

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ENERGY Client: Cotter Corporation Project: Schwartz GW 4/24/12 S26350 Method: E200.8 Sample ID: LFB Manganese Phosphorus Silver Thallium Method: E200.8 Sample ID: ICV Aluminum Iron Zinc www.energylab.com Mafytlnl Excitors Sou 1857 8 Laboratory Fortified Blank 0.0556 mg /L 1.31 mg /L 0.0212 mg /L 0.0534 mg /L 3 Initial Calibration Verification Standard Method: E200.8 Sample ID: LRB 3 Method Blank Aluminum ND mg /L 0.0002 Iron ND mg /L 0.0006 Zinc ND mg /L 0.0002 Qualifiers: RL - Analyte reporting limit. MDC - Minimum detectable concentration Helena, MT 817- 472 -0711 • Billings, MT 800- 735 -4489 • Casper, WY 888- 235 -0515 Gillette, WY 866- 686 -7175 • Rapid City, SD 888- 672 -1225 • College Station, TX 888- 690 -2218 QA/QC Summary Report Prepared by Casper, WY Branch Run: ICPMS4- C_120501 B 0.0010 111 85 115 0.0024 105 85 115 0.0010 105 85 115 0.0010 107 85 115 0.0477 mg /L 0.0010 95 90 110 0.981 mg /L 0.0010 98 90 110 0.0488 mg /L 0.0010 98 90 110 Run: ICPMS4-C_120502A Sample ID: LFB 3 Laboratory Fortified Blank Run: ICPMS4- C_120502A Aluminum 0.0491 mg /L 0.0010 98 85 115 Iron 1.22 mg /L 0.0010 98 85 115 Zinc 0.0499 mg /L 0.0010 100 85 115 Sample ID: C12041294- 003CMS4 3 Sample Matrix Spike Run: ICPMS4- C_120502A Aluminum 0.0552 mg /L 0.030 105 70 130 Iron 1.28 mg /L 0.030 102 70 130 Zinc 0.0540 mg /L 0.010 104 70 130 ND - Not detected at the reporting limit. Report Date: 06/06/12 Work Order: C12041245 Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Analytical Run: ICPMS4- C_120502A 05/02/12 11:40 Page 10 of 19 Batch: R159156A 05/01/12 18:00 Batch: R159174A 05/02/12 12:16 05/02/12 12:21 05/02/12 14:41 Sample ID: C12041294- 003CMSD 3 Sample Matrix Spike Duplicate Run: ICPMS4- C_120502A 05/02/12 14:46 Aluminum 0.0553 mg /L 0.030 105 70 130 0.3 20 Iron 1.32 mg /L 0.030 105 70 130 2.8 20 Zinc 0.0549 mg /L 0.010 106 70 130 1.6 20