2012-08-06_HYDROLOGY - M1977300 (3)

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ENERGY Qualifiers: Client: Cotter Corporation Analyte Method: E200.8 Sample ID: C12050704- 002BMS4 Aluminum Antimony Calcium Copper Iron Magnesium Molybdenum Potassium Silver Sodium Thallium www.energylab.com Aatlydesl ExosAYecr S1Doe 1852 11 Sample Matrix Spike 0.0714 mg /L 0.0532 mg /L 15.8 mg /L 0.0501 mg /L 1.28 mg /L 13.2 mg /L 0.0518 mg /L 15.0 mg /L 0.0189 mg /L 110 mg /L 0.0489 mg /L Helena, MT 677 - 412 - 0711 • Billings, MT 800 - 735 - 4489 • Casper, WY 888 235 - 0515 Gillette, WY 866 - 686 - 7175 • Rapid City, SO 888 672 - 1225 • College Station, TX 888 - 690 - 2218 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 06/13/12 Project: Schwartz - SW 5/10/11 S26366- S26368 Work Order: 012050482 Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Quai Method: E200.8 Analytical Run: ICPMS4- C_120521A Sample ID: ICV 11 Initial Calibration Verification Standard 05/21/12 15:48 Aluminum 0.0472 mg /L 0.0010 94 90 110 Antimony 0.0495 mg /L 0.0010 99 90 110 Calcium 10.2 mg /L 0.0066 102 90 110 Copper 0.0510 mg /L 0.0010 102 90 110 Iron 1.08 mg /L 0.0010 108 90 110 Magnesium 10.0 mg /L 0.0027 100 90 110 Molybdenum 0.0497 mg /L 0.0010 99 90 110 Potassium 9.91 mg /L 0.0041 99 90 110 Silver 0.0203 mg /L 0.0010 102 90 110 Sodium 10.0 mg /L 0.0043 100 90 110 Thallium 0.0476 mg /L 0.0010 95 90 110 Run: ICPMS4-C_120521A 0.030 107 70 130 0.0010 106 70 130 1.0 101 70 130 0.0050 99 70 130 0.030 101 70 130 1.0 104 70 130 0.0010 100 70 130 1.0 100 70 130 0.0010 94 70 130 1.0 70 130 0.00050 98 70 130 Sample ID: C12050704 -002BMSD 11 Sample Matrix Spike Duplicate Run: ICPMS4- C_120521A 05/21/12 18:20 Aluminum 0.0718 mg /L 0.030 108 70 130 0.7 20 Antimony 0.0525 mg /L 0.0010 105 70 130 1.4 20 Calcium 15.4 mg /L 1.0 98 70 130 2.6 20 Copper 0.0493 mg /L 0.0050 97 70 130 1.8 20 Iron 1.25 mg /L 0.030 100 70 130 1.8 20 Magnesium 12.9 mg /L 1.0 102 70 130 2.1 20 Molybdenum 0.0517 mg /L 0.0010 99 70 130 0.3 20 Potassium 14.5 mg /L 1.0 97 70 130 2.8 20 Silver 0.0187 mg /L 0.0010 93 70 130 1.0 20 Sodium 109 mg /L 1.0 70 130 1.1 20 A Thallium 0.0480 mg /L 0.00050 96 70 130 1.9 20 Sample ID: LRB 11 Method Blank Run: ICPMS4- C_120521 A Aluminum ND mg /L 0.0002 Antimony ND mg /L 0.0001 Calcium ND mg /L 0.007 Copper ND mg /L 3E -05 Iron ND mg /L 0.0006 RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. ND - Not detected at the reporting limit. MDC - Minimum detectable concentration Page 17 of 30 Batch: R159869a 05/21/12 18:16 A 05/21/12 16:23