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ENERGY <br />Analyte <br />Sample ID: LCS3 -33549 <br />Aluminum <br />Antimony <br />Chromium <br />Copper <br />Iron <br />Lead <br />Manganese <br />Molybdenum <br />Thallium <br />Uranium <br />Zinc <br />Client: Cotter Corporation <br />Sample ID: C12050084 -002DMS3 <br />Aluminum <br />Antimony <br />Chromium <br />Copper <br />Iron <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energylab.com <br />AealytkalExcukem Sine 1152 <br />11 Sample Matrix Spike <br />2.62 mg /L <br />0.553 mg /L <br />0.536 mg /L <br />0.508 mg /L <br />2.79 mg /L <br />Helena, MT 877.472 -0711 • Billings, MT 800-735-4489 • Casper, WY 888 -235 -0515 <br />Gillette, WY 888 -686 -7175 • Rapid City, SD 888- 672 -1225 • College Station, TX 888 - 608 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Method: E200.8 <br />Sample ID: MB -33549 11 Method Blank <br />Aluminum 0.001 mg /L 0.001 <br />Antimony 0.0002 mg /L 0.0001 <br />Chromium 0.0006 mg /L 1E-05 <br />Copper 0.0009 mg /L 2E -05 <br />Iron 0.003 mg/L 0.0008 <br />Lead 2E -05 mg /L 1E-05 <br />Manganese 0.0001 mg /L 4E -05 <br />Molybdenum 0.0005 mg /L 4E -05 <br />Thallium ND mg /L 3E -05 <br />Uranium 2E -05 mg /L 8E -06 <br />Zinc 0.001 mg /L 0.0002 <br />11 Laboratory Control Sample <br />2.64 mg /L <br />0.569 mg /L <br />0.530 mg /L <br />0.512 mg /L <br />2.57 mg /L <br />0.553 mg /L <br />2.81 mg /L <br />0.524 mg /L <br />0.524 mg /L <br />0.546 mg /L <br />0.516 mg /L <br />Run: ICPMS4- C_120504A <br />Run: I C P M S 4- C_120504A <br />0.030 106 85 115 <br />0.0010 114 85 115 <br />0.0050 106 85 115 <br />0.0050 102 85 115 <br />0.030 103 85 115 <br />0.0010 111 85 115 <br />0.0010 112 85 115 <br />0.0010 105 85 115 <br />0.00050 105 85 115 <br />0.00030 109 85 115 <br />0.010 103 85 115 <br />Run: ICPMS4 -C 120504A <br />0.030 102 70 130 <br />0.0010 111 70 130 <br />0.0050 107 70 130 <br />0.0050 101 70 130 <br />0.030 106 70 130 <br />ND - Not detected at the reporting limit. <br />Report Date: 06/11/12 <br />Project: Schwartz SW 5/01/12 S26376 & S26383 Work Order: C12050084 <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.8 Analytical Run: ICPMS4- C_120504A <br />Sample ID: ICV 11 Initial Calibration Verification Standard 05/04/12 11:58 <br />Aluminum 0.0502 mg /L 0.0010 100 90 110 <br />Antimony 0.0482 mg /L 0.0010 96 90 110 <br />Chromium 0.0493 mg /L 0.0010 99 90 110 <br />Copper 0.0496 mg /L 0.0010 99 90 110 <br />Iron 1.02 mg /L 0.0010 102 90 110 <br />Lead 0.0488 mg /L 0.0010 98 90 110 <br />Manganese 0.0492 mg /L 0.0010 98 90 110 <br />Molybdenum 0.0488 mg /L 0.0010 98 90 110 <br />Thallium 0.0473 mg /L 0.0010 95 90 110 <br />Uranium 0.0463 mg /L 0.00030 93 90 110 <br />Zinc 0.0502 mg /L 0.0010 100 90 110 <br />Page 16 of 29 <br />Batch: 33549 <br />05/04/12 14:43 <br />05/04/12 14:47 <br />05/04/12 16:37 <br />