2012-08-06_HYDROLOGY - M1977300 (3)

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ENERGY Client: Cotter Corporation www.energylab corn Ambers!Eralksee Skye 1952 Method: E200.8 Sample ID: C12050094 -004BMS4 Aluminum Antimony Calcium Copper Iron Magnesium Manganese Potassium Sodium Thallium Uranium Zinc Analyte Count Result Units 12 Sample Matrix Spike 0.0560 mg /L 0.0526 mg /L 26.6 mg /L 0.0468 mg /L 1.27 mg /L 13.9 mg /L 0.0674 mg /L 14.3 mg /L 151 mg /L 0.0497 mg /L 0.0552 mg /L 0.0545 mg /L Sample ID: LRB 12 Method Blank Aluminum ND mg /L Antimony ND mg /L Qualifiers: Helena, K1877472 • Billings, MT 800-735-4489 • Casper, WY 888- 235 -0515 Gilhtte, WY 818-688-7175 • Rapid City, SD 888 - 672 -1225 • College Station, TX 888 - 600 -2218 QA/QC Summary Report Prepared by Casper, WY Branch Report Date: 06/11/12 Project: Schwartz SW 5/01/12 S26376 & S26383 Work Order: C12050084 RL %REC Low Limit High Limit RPD RPDLImit Qual Method: E200.8 Analytical Run: ICPMS4- C_120503A Sample ID: ICV 12 Initial Calibration Verification Standard 05/03/12 11:34 Aluminum 0.0493 mg /L 0.0010 99 90 110 Antimony 0.0496 mg /L 0.0010 99 90 110 Calcium 9.75 mg /L 0.0066 98 90 110 Copper 0.0517 mg /L 0.0010 103 90 110 Iron 1.04 mg /L 0.0010 104 90 110 Magnesium 9.53 mg /L 0.0027 95 90 110 Manganese 0.0494 mg /L 0.0010 99 90 110 Potassium 9.92 mg /L 0.0041 99 90 110 Sodium 9.40 mg /L 0.0043 94 90 110 Thallium 0.0475 mg /L 0.0010 95 90 110 Uranium 0.0486 mg /L 0.00030 97 90 110 Zinc 0.0517 mg /L 0.0010 103 90 110 Run: ICPMS4- C1 20503A 0.030 106 70 130 0.0010 105 70 130 1.0 102 70 130 0.0050 94 70 130 0.030 101 70 130 1.0 100 70 130 0.0010 109 70 130 1.0 96 70 130 1.0 70 130 0.00050 99 70 130 0.00030 109 70 130 0.010 105 70 130 Batch: R159247A 05/03/12 14:36 A Sample ID: C12050094 -004BMSD 12 Sample Matrix Spike Duplicate Run: ICPMS4- C_120503A 05/03/12 14:41 Aluminum 0.0563 mg /L 0.030 106 70 130 0.5 20 Antimony 0.0534 mg /L 0.0010 107 70 130 1.6 20 Calcium 27.5 mg /L 1.0 110 70 130 3.4 20 Copper 0.0487 mg /L 0.0050 97 70 130 4.0 20 Iron 1.31 mg /L 0.030 104 70 130 3.0 20 Magnesium 14.5 mg /L 1.0 105 70 130 4.4 20 Manganese 0.0670 mg /L 0.0010 108 70 130 0.5 20 Potassium 14.9 mg /L 1.0 101 70 130 4.1 20 Sodium 158 mg /L 1.0 70 130 4.5 20 A Thallium 0.0501 mg /L 0.00050 100 70 130 0.7 20 Uranium 0.0548 mg /L 0.00030 109 70 130 0.6 20 Zinc 0.0571 mg /L 0.010 110 70 130 4.6 20 0.0002 0.0001 Run: ICPMS4-C_120503A 05/03/12 12:11 RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. ND - Not detected at the reporting limit. MDC - Minimum detectable concentration Page 14 of 29