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ENERGY <br />Client: Cotter Corporation <br />Project: Schwartz GW 4/27/12 S26359 <br />Analyte <br />Method: E300.0 <br />Sample ID: ICV- 043012 -10 <br />Chloride <br />Method: E300.0 <br />Sample ID: ICB- 043012 -11 <br />Chloride <br />Sample ID: LFB -043012 -12 <br />Chloride <br />Sample ID: C12041237 -001AMS <br />Chloride <br />- Matrix spike recoveries outside the accep <br />Sample ID: C12041237 -001AMSD <br />Chloride <br />- Matrix spike recoveries outside the acceptance range are considered matrix - related. <br />Method: E300.0 <br />Sample ID: ICV- 050212 -10 <br />Sulfate <br />Method: E300.0 <br />Sample ID: ICB2- 050212 -11 <br />Sulfate <br />Sample ID: LFB- 050212 -12 Laboratory Fortified Blank <br />Sulfate <br />Sample ID: LFBD- 050212 -13 Laboratory Fortified Blank Duplicate <br />Sulfate <br />Sulfate <br />www.energylab.com <br />Aa bWealExcelenceSive 1152 <br />Count Result Units <br />Initial Calibration Verification Standard <br />9.98 mg /L 1.0 100 <br />Method Blank <br />ND mg /L <br />Laboratory Fortified Blank <br />9.99 mg /L <br />Sample Matrix Spike <br />187 mg /L <br />tance range are considered matrix - related. <br />Sample Matrix Spike Duplicate <br />190 mg /L <br />Method Blank <br />0.1 mg /L <br />39.8 mg /L <br />39.8 mg /L <br />Sample ID: C12041332- 001BMS Sample Matrix Spike <br />Initial Calibration Verification Standard <br />40.1 mg /L 1.0 100 <br />1450 mg /L <br />- Matrix spike recoveries outside the acceptance range are considered matrix - related. <br />Sample ID: C12041332 -001BMSD Sample Matrix Spike Duplicate <br />Sulfate 1460 mg /L <br />- Matrix spike recoveries outside the acceptance range are considered matrix - related. <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />Helene, MT 877472 -0711 • Billings, MT 800 -135 -4488 • Casper, WY 888- 235 -0515 <br />Gillette, WY 868 -688 -1175 • Rapid City, SD 888- 672 -1225 • College Station, TX 888 -610 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />RL %REC Low Limit High Limit RPD RPDLImIt Qua! <br />Run: IC2- C_120430A <br />0.03 <br />Run: IC2- C_120430A <br />1.0 100 90 110 <br />Run: IC2- C_120430A <br />1.0 85 90 110 <br />Run: IC2- C_120430A <br />1.0 90 90 110 <br />90 <br />90 <br />Run: IC2- C_120503A <br />110 <br />110 <br />Run: IC2- C_120503A <br />99 90 110 <br />Run: IC2- C_120503A <br />99 90 110 <br />Run: IC2- C_120503A <br />89 90 110 <br />ND - Not detected at the reporting limit. <br />S - Spike recovery outside of advisory limits. <br />Report Date: 06/06/12 <br />Work Order: C12041332 <br />Analytical Run: IC2- C_120430A <br />04/30/12 14:45 <br />Batch: R159160 <br />04/30/12 15:01 <br />04/30/12 15:48 <br />05/01/12 15:37 <br />S <br />05/01/12 15:52 <br />1.2 10 <br />Analytical Run: IC2- C_120503A <br />05/02/12 17:03 <br />Run: 1C2- C_120503A 05/02/12 22:58 <br />8.0 92 90 110 0.7 10 <br />Page 11 of 19 <br />Batch: R159204 <br />05/02/12 17:18 <br />05/02/12 17:34 <br />05/02/12 17:49 <br />05/02/12 22:42 <br />S <br />