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Table 9-5-1 <br /> Parameters and Analytical Procedures Utilized for Topsoil Analysis <br /> Parameter-Units Procedure-Reference <br /> Sample Preparation Samples were air dried at less than 35' C. Clods <br /> were broke up prior to grinding and sieving of <br /> sample. Large coarse fragments were removed. Sample <br /> material was sieved. Remaining rock coarse fragments <br /> left on the 10 mesh (2 mm) sieve were removed. <br /> Remaining soil clods left on the 10 mesh screen were <br /> ground until the sample just passed the screen. <br /> Excessive grinding of sample material was avoided <br /> during the entire sample preparation procedure. <br /> Subsampling of sieved (less than USDA Handbook 60, 1954 Diagnosis and Improvement <br /> 2 mm) soil materials for analysis of Saline and Alkali Soils. pp. 83-84. U.S. <br /> Salinity Laboratory Staff. <br /> Coarse fragment content, USDA Handbook 436, Soil Taxonomy. App. I, pg. 472; <br /> percent by weight Soil Survey Laboratory Methods and Procedures for <br /> Collecting Soil Samples, pages 9 and 12-13. <br /> pH USDA Handbook 60, Method (21A), page 102, and page <br /> 84: Method (2). <br /> Conductivity in USDA Handbook 60, Method (3a), page 84, and Method <br /> mmhos/cm @ 25' C (4b) pages 89-90. <br /> Preparation of saturation USDA Handbook 60, Methods 2 and 3a, pages 84 and 88, <br /> extract and saturation and 27a and b, page 107. <br /> percent determination <br /> Particle-Size Analysis in Hydrometer Method. ASA Mono. No. 9, part. 1, <br /> Percent. clay, silt, sand, Method 43-5, pages 562-566. Two hour and 8-hour <br /> and very fine sand settling times were used for clay. Sieve analysis <br /> (vfs = 0.05-0.lmm) used for vfs (140-270) mesh. ASA Mono. No. 9, Part 1 <br /> pages 554-556. Black, 1965 and 1982. <br /> Texture USDA Handbook 18, pages 205-223. <br /> Soluble Ca, Mg, and Na, meq/1 Extraction of Ca, Mg, and Na by USDA Handbook 60, <br /> Method (3a), page 84. Analysis by atomic adsorption <br /> spectrophotometry. <br /> Sodium-Adsorption Ratio USDA Handbook 60, page 26. <br /> Carbonates, Percent USDA Handbook 60, Method (23c), page 105. <br /> Organic Matter, Percent A.S.A. Monograph No. 9, 1982, Part 2, Method <br /> 29-3.5.2, page 570. <br /> 9-5-13 Revised 04/11/88 <br />