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November 16, 2011 <br />New Elk Coal Company <br />122 West First St. <br />Trinidad, CO 81082 <br />USA <br />Client Sample ID: <br />Date Received: <br />Matrix: <br />PAW -9 (NE 050D) <br />11/04/2011 <br />Ground Water <br />TESTS RESULT <br />Chloride, Total 16 mg /L <br />Conductivity 510 umhos /cm <br />Arsenic, Dissolved <0,002 mg /L <br />Cadmium, Dissolved <0.0002 mg /L <br />Lead, Dissolved <0.001 mg /L <br />Selenium, Dissolved <0.002 mg /L <br />Silver, Dissolved <0.0002 mg /L <br />Chromium, Dissolved <0.005 mg(L <br />Copper, Dissolved <0.005 mg /L <br />Iron, Dissolved <0.01 mg /L <br />Manganese, Dissolved 0.11 mg /L <br />Nickel, Dissolved <0.01 mg /L <br />Zinc, Dissolved 0.007 mg /L <br />Nitrogen, Nitrate /Nitrite 0.20 mg/L N <br />pH 7.59 s.u. <br />pH Temperature 18.0 °C <br />Solids, Total Dissolved 420 mg /L <br />Sulfate 47 mg /L <br />Method Reference(s): <br />Analysis Report <br />SGS Minerals Sample ID: 072 - 56860 -004 <br />REPORTING <br />METHOD LIMIT <br />EPA300.0 1 <br />SM2510 B 1 <br />EPA200.9 0.002 <br />EPA200.9 0.0002 <br />EPA200.9 0.001 <br />EPA200.9 0.002 <br />EPA200.9 0.0002 <br />EPA200.7 0.005 <br />EPA200.7 0.005 <br />EPA200.7 0.01 <br />EPA200.7 0.005 <br />EPA200.7 0.01 <br />EPA200.7 0.005 <br />EPA300.0 0.02 <br />SM4500 -H B 0.01 <br />SM4500 -H B <br />SM2540 C 5 <br />EPA300.0 5 <br />"Standard Methods for the Examination of Water and Wastewater ", 18th Edition, 1992; APHA - AWWA -WEF <br />"Methods for the Determination of Metals in Environmental Samples ", EPA/600 /4- 91/010, June 1991 <br />"Methods for the Determination of Inorganic Substances in Environmental Samples ", EPA/600 /R- 931100 <br />Date Sampled <br />Project Name/# : <br />Sample Type : <br />11/03/2011 <br />Table 1 NPDES List 5 <br />Grab <br />ANALYZED <br />DATE / TIME <br />11/04/2011 1545 <br />11/09/2011 2011 <br />11/06/2011 1000 <br />11/08/2011 1500 <br />11/07/2011 0900 <br />11/06/2011 1600 <br />11/09/2011 1200 <br />11/07/2011 0925 <br />11/07/2011 0925 <br />11/07/2011 0925 <br />11/07/2011 0925 <br />11(07/2011 0925 <br />11/07/2011 0925 <br />11/04/2011 1545 <br />11/4 /11 1600 <br />11/4 /11 1600 <br />11/10/11 1600 <br />11/04/2011 1545 <br />Page 1 of 1 <br />ANALYST <br />ST <br />IJ <br />CSK <br />EH <br />CSK <br />CSK <br />DM <br />EH <br />EH <br />EH <br />EH <br />EH <br />EH <br />ST <br />JT <br />JT <br />JT <br />ST <br />Somer Rodriguez, Denver Laboratory <br />SOS North America Inc. Minerals Services Division <br />4665 Paris St Suite B -200 Denver CO 80239 t (303) 373 -4772 f (303) 373 -4791 www.sys.com /minerals <br />Member of SGS Group <br />This document Is issued by the Company under its General Conditions of Service accessible at http: / /www,sgs.comfterms and_condltions.htm Attention is <br />drawn to the limitation of liability, Indemnification end jurisdiction Issues defined therin. <br />Any holder of this document Is advised that Information contained hereon reflects the Company's findings at the time of Its intervention only and within the limits <br />of Client's instructions, if any. The Company's sole responsibility is to its client and this document does not exonerate parties to a transaction from exercising all <br />their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document <br />is unlawful and offenders may be prosecuted to the fullest extent of the law. <br />