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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />St. Sophia Holding Ltd. <br />Project ID: <br />Sample ID: <br />Wet Chemistry <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL Date Analyst <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Biochemical Oxygen <br />Demand (5 day) <br />Chemical Oxygen <br />Demand <br />Chloride <br />Chromium, Hexavalent <br />Coliforms, fecal <br />Cyanide, total <br />Cyanide, WAD <br />Fluoride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Nitrogen, ammonia <br />Nitrogen, organic <br />Nitrogen, total Kjeldahl <br />pH (lab) <br />pH <br />pH measured at <br />Phenol <br />Phosphorus, total <br />Residue, Filterable <br />(TDS) @180C <br />Residue, Non - <br />Filterable (TSS) <br />@105C <br />Sulfate <br />Sulfide as S <br />LMTCDPS001- 071111 <br />SM2320B - Titration <br />SM5210B <br />M410.4 <br />SM4500CI -E <br />SM3500Cr -D <br />SM9222D - Membrane Filter <br />M335.4 - Colorimetric w/ <br />distillation <br />SM4500 -CN I- Colorimetric w/ <br />distillation <br />SM4500F -C <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 0.06 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />M350.1 - Automated Phenate <br />M351.2 & M350.1 - TKN minus <br />NH3 <br />M351.2 - TKN by Block Digester <br />SM4500H+ B <br />420.4, Manual Distillation <br />M365.1 - Auto Ascorbic Acid <br />(digest) <br />SM2540C <br />SM2540D <br />D516 -02 - Turbidimetric <br />376.2 - Methylene Blue <br />47 <br />U mg /L <br />U mg /L <br />47 mg /L <br />U • mg /L <br />24 <br />0.2 <br />79 <br />0.06 <br />U <br />U <br />HU <br />H <br />U <br />U <br />B <br />B <br />B <br />U <br />U <br />U <br />8.0 H <br />20.0 <br />0.005 B <br />0.01 B <br />38 <br />U <br />U <br />mg /L <br />mg /L <br />#/100m1 <br />mg /L <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />mg /L 0.003 0.01 <br />mg /L 1 <br />U mg /L 0.01 0.05 <br />mg /L 0.05 0.5 <br />mg /L 0.1 0.5 <br />mg /L 0.1 0.5 <br />units <br />C <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />Inorganic Analytical <br />Results <br />mg /L 2 20 07/13/11 0:00 <br />2 20 07/13/11 0:00 <br />2 20 07/13/11 0:00 <br />2 20 07/13/11 0:00 <br />2 2 07/13/11 11:50 <br />mg /L 10 20 07/15/11 15:17 cra <br />1 <br />0.005 <br />1 <br />0.003 <br />0.1 <br />0.1 <br />0.003 <br />0.01 <br />5 <br />0.02 <br />5 <br />0.01 <br />L89127 -02 <br />07/11/11 12:30 <br />07/12/11 <br />Waste Water <br />07/29/11 13:51 <br />07/12/11 15:30 <br />07/12/11 15:10 <br />07/15/11 22:33 <br />07/23/11 14:30 pjb . <br />mg /L 0.1 0.5 07/22/11 12:06 <br />7 08/15/11 16:18 <br />07/15/11 12:19 <br />07/20/11 10:25 <br />cra <br />cra <br />cra <br />cra <br />cra <br />mpb <br />ndm <br />cra <br />pjb <br />abm <br />calc <br />ndm <br />mfm <br />mg /L 0.02 0.1 08/15/11 16:18 calc <br />mg /L 0.02 0.1 07/12/11 20:12 pjb <br />0.1 <br />0.1 <br />0.02 <br />0.05 <br />07/12/11 20:12 pjb <br />07/29/11 18:52 lhb <br />08/15/11 16:18 calc <br />07/30/11 14:57 pjb <br />07/13/11 0:00 <br />07/13/11 0:00 <br />07/16/11 16:57 <br />07/29/11 21:44 <br />cra <br />cra <br />pjb <br />pjb <br />120 mg /L 10 20 07/13/11 16:16 ndm <br />mg /L 5 20 07/14/11 14:26 cra <br />5 30 08/01/11 10:44 <br />0.02 0.1 07/13/11 16:25 <br />ccp <br />las <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 8 of 68 <br />