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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />ACZ Sample ID: <br />L84991 -02 <br />Kerr Coal Company Date Sampled: <br />10120/10 12:20 <br />Project ID: Date Received: <br />10121110 <br />Sample ID: AP -2 <br />Sample Matrix: <br />Ground Water <br />Field Data <br />Conductivity (Field) Field Measurement <br />pH (Field) Field Measurement <br />Temperature (Field) Field Measurement <br />Metals Analysis <br />Calcium, dissolved M200.7 ICP <br />Iron, dissolved <br />M200.7 ICP <br />Magnesium, dissolved <br />M200.7 ICP <br />Manganese, dissolved <br />M200.7 ICP <br />Potassium, dissolved <br />M200.7 ICP <br />Sodium, dissolved <br />M200.7 ICP <br />Wet Chemistry <br />Calculation <br />Alkalinity as CaCO3 SM2320B - Titration <br />Bicarbonate as <br />mg /L 0 <br />CaCO3 <br />1 1 <br />Carbonate as CaCO3 <br />ear <br />Hydroxide as CaCO3 <br />mg /L 0 <br />Total Alkalinity <br />0.05 1 <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />mg /L 0 <br />Sum of Anions <br />1 1 <br />Sum of Cations <br />ear <br />Chloride <br />SM4500CI -E <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />Lab Filtration <br />SM 3030 B <br />Lab Filtration & <br />SM 3030 B <br />Acidification <br />Nitrate as N, dissolved <br />Calculation: NO3NO2 minus NO2 <br />Nitrate/Nitrite as N, <br />M353.2 - Automated Cadmium <br />dissolved <br />Reduction <br />Nitrite as N, dissolved <br />M353.2 - Automated Cadmium <br />10/29/1011:39 e <br />Reduction <br />Residue, Filterable <br />SM2540C <br />(TDS) @180C <br />Sodium Absorption <br />USGS 11738 78 <br />Ratio in Water <br />Sulfate <br />SM4500 SO4 -D <br />TDS (calculated) <br />Calculation <br />TDS (ratio - <br />Calculation <br />measured/calculated) <br />20 1 <br />600 <br />umhos /cm 10/20/1012:20 jm <br />7.9 units 10/20/10 12:20 im <br />12.0 C 10/20/1012:20 jm <br />' Please refer to Qualifier Reports for details. <br />REPIN.02.06.05.01 <br />Page 3 of 10 <br />mg /L 0 <br />0.2 1 <br />1 1 <br />10/2811018:44 e <br />ear <br />43.7 m <br />mg /L 0 <br />0.02 0 <br />0.05 1 <br />10/28/1018:44 e <br />ear <br />0.20 m <br />mg /L 0 <br />0.2 1 <br />1 1 <br />10/28/1018:44 e <br />ear <br />31.2 m <br />mg /L 0 <br />0.005 0 <br />0.03 1 <br />10/28/1018:44 e <br />ear <br />0.132 m <br />B mg /L 0 <br />0.3 2 <br />2 1 <br />10/29/1011:39 e <br />ear <br />1.5 B <br />mg /L 0 <br />0.3 2 <br />2 1 <br />10/29/1011:39 e <br />ear <br />25.5 m <br />mg /L 2 <br />2 2 <br />20 1 <br />10/23/10 0:00 I <br />Ihb <br />284 m <br />B mg /L 2 <br />2 2 <br />20 1 <br />10/23/10 0:00 I <br />Ihb <br />8 B <br />U mg /L 2 <br />2 2 <br />20 1 <br />10/23/10 0:00 I <br />Ihb <br />mg /L 2 <br />2 2 <br />20 1 <br />10/23/10 0:00 I <br />Ihb <br />292 m <br />11/02/1011:19 c <br />calc <br />-5.6 1 <br />meq /L 0 <br />0.1 0 <br />0.5 1 <br />11/02/1011:19 c <br />calc <br />6.6 m <br />meq /L 0 <br />0.1 0 <br />0.5 1 <br />11/02/1011:19 c <br />calc <br />5.9 m <br />mg /L 1 <br />1 <br />5 1 <br />11/01/1013:05 i <br />itk <br />6 m <br />mg /L 1 <br />1 7 <br />7 <br />11 /02/10 11:19 t <br />talc <br />237 m <br />• 1 <br />10/21/1014:19 a <br />abm <br />10/21/10 14:35 a <br />abm <br />B mg /L 0 <br />0.02 0 <br />0.1 1 <br />11/02/1011:19 c <br />calc <br />0.06 B <br />B ' mg /L 0 <br />0.02 0 <br />0.1 1 <br />10/21/10 21:08 p <br />pjb <br />0.06 B <br />U mg /L 0 <br />0.01 0 <br />0.05 1 <br />10 /21 /10 21:08 p <br />pjb <br />mg /L 1 <br />10 2 <br />20 1 <br />10/22/1012:33 a <br />abm <br />340 m <br />0.03 0 <br />0.15 1 <br />11/02/10 11:19 c <br />calc <br />0.72 0 <br />B mg /L 1 <br />10 5 <br />50 1 <br />10/29/1011:02 a <br />abm <br />30 B <br />mg /L 1 <br />10 5 <br />50 1 <br />11/02/1011:19 c <br />calc <br />317 m <br />11/02/1011:19 c <br />calc <br />107 <br />' Please refer to Qualifier Reports for details. <br />REPIN.02.06.05.01 <br />Page 3 of 10 <br />