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ENERGY <br />Client: Cotter Corporation <br />Project: Schwartz SW 08/17/11 S25909- S25916 <br />wwwanetgylab com Helena, MT 877 - 472 -0711 • Billings, MT 800 -735 -4489 • Casper, WY 888- 235 -0515 <br />Asittleal Engle= SNIP 7152 Gillette, WY 886 -686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888 -690 -2218 <br />Analyte <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.8 <br />Sample ID: C11080845- 005BMS4 12 Sample Matrix Spike <br />Aluminum 5.12 mg /L <br />Antimony 5.05 mg /L <br />Arsenic 5.93 mg /L <br />Boron 13.3 mg /L <br />Chromium 4.87 mg /L <br />Iron 117 mg /L <br />Lead 5.08 mg /L <br />Manganese 4.74 mg /L <br />Molybdenum 626 mg /L <br />Silver 1.80 mg /L <br />Thallium 5.10 mg /L <br />Zinc 4.68 mg /L <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Sample ID: LRB 12 Method Blank <br />Aluminum ND mg /L 8E -05 <br />Antimony ND mg /L 0.0002 <br />Arsenic ND mg /L 4E -05 <br />Boron 0.0004 mg /L <br />Chromium ND mg /L 5E -05 <br />Iron ND mg /L 0.0001 <br />Lead ND mg /L 2E -05 <br />Manganese ND mg /L 2E -05 <br />Molybdenum ND mg /L 8E -05 <br />Silver 0.0002 mg /L 8E -05 <br />Thallium ND mg /L 2E -05 <br />Zinc ND mg /L 0.0001 <br />Qualifiers: <br />Run: ICPMS4 -C 110825A <br />0.10 102 70 130 <br />0.050 101 70 130 <br />0.0042 97 70 130 <br />0.10 79 70 130 <br />0.050 97 70 130 <br />0.030 94 70 130 <br />0.050 102 70 130 <br />0.010 95 70 130 <br />0.10 70 130 <br />0.010 90 70 130 <br />0.10 102 70 130 <br />0.012 88 70 130 <br />Sample ID: LFB 12 Laboratory Fortified Blank Run: ICPMS4- C_110825A <br />Aluminum 0.0505 mg /L 0.0010 101 85 115 <br />Antimony 0.0489 mg /L 0.0010 98 85 115 <br />Arsenic 0.0487 mg /L 0.0010 97 85 115 <br />Report Date: 09/29/11 <br />Work Order: C11080832 <br />Page 20 of 39 <br />Batch: R149824A <br />08/25/11 14:58 <br />A <br />Sample ID: C11080845- 005BMSD 12 Sample Matrix Spike Duplicate Run: ICPMS4- C_110825A 08/25/11 15:02 <br />Aluminum 5.09 mg /L 0.10 102 70 130 0.7 20 <br />Antimony 5.10 mg /L 0.050 102 70 130 1.1 20 <br />Arsenic 6.36 mg /L 0.0042 106 70 130 7.0 20 <br />Boron 14.6 mg /L 0.10 106 70 130 9.6 20 <br />Chromium 5.01 mg /L 0.050 100 70 130 2.9 20 <br />Iron 118 mg /L 0.030 94 70 130 0.3 20 <br />Lead 5.13 mg /L 0.050 103 70 130 0.9 20 <br />Manganese 4.74 mg /L 0.010 95 70 130 0.0 20 <br />Molybdenum 703 mg /L 0.10 70 130 12 20 A <br />Silver 1.81 mg /L 0.010 90 70 130 0.5 20 <br />Thallium 5.11 mg /L 0.10 102 70 130 0.2 20 <br />Zinc 4.71 mg /L 0.012 89 70 130 0.6 20 <br />Run: ICPMS4 -C 110825A 08/25/11 11:47 <br />08/25/11 11:52 <br />RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In <br />accordance with the method % recovery is not calculated. <br />ND - Not detected at the reporting limit. MDC - Minimum detectable concentration <br />