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ENERGY <br />Method: E300.0 <br />Sample ID: ICV081211 <br />Chloride <br />Sulfate <br />Sample ID: ICB2081211 <br />Chloride <br />Sulfate <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energyleb.com <br />MOAN, Exeamen= 1952 <br />Client: Cotter Corporation <br />Project: Schwartz SW 8/10/11 S25161- S25163 <br />Helena, MI 877 -472 -0711 • Billings, MT 800- 735 -4489 • Casper, WY 888- 235 -0515 <br />Gillette, WY 886 -686 -7175 • Rapid City, SD 888 - 672 -1225 • College station, 7X 888 -690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />2 Initial Calibration Verification Standard <br />10.4 mg /L <br />40.8 mg /L <br />2 Initial Calibration Blank, Instrument Blank <br />- 0.0110 mg /L <br />0.128 mg /L <br />1.0 104 90 110 <br />1.0 102 90 110 <br />1.0 <br />1.0 <br />Method: E300.0 <br />Sample ID: ICB081211 2 Method Blank <br />Chloride ND mg /L 0.04 <br />Sulfate 0.1 mg /L 0.1 <br />0 <br />0 <br />Run: IC2- C_110812A <br />0 <br />0 <br />Sample ID: LFB081211 2 Laboratory Fortified Blank Run: IC2- C_110812A <br />Chloride 10.6 mg /L 1.0 106 90 110 <br />Sulfate 41.4 mg /L 1.0 103 90 110 <br />Sample ID: LFBD081211 2 Laboratory Fortified Blank Duplicate Run: IC2- C_110812A 08/12/11 17:43 <br />Chloride 10.6 mg /L 1.0 106 90 110 0.4 10 <br />Sulfate 41.3 mg /L 1.0 103 90 110 0.1 10 <br />Sample ID: C11080487- 004AMS 2 Sample Matrix Spike Run: IC2- C_110812A <br />Chloride 12.6 mg /L 1.0 102 80 120 <br />Sulfate 54.1 mg /L 1.0 102 80 120 <br />Sample ID: C11080487- 004AMSD 2 Sample Matrix Spike Duplicate Run: IC2- C_110812A 08/13/11 06:34 <br />Chloride 12.9 mg /L 1.0 106 80 120 2.8 10 <br />Sulfate 55.4 mg /L 1.0 106 80 120 2.4 10 <br />ND - Not detected at the reporting limit. <br />Report Date: 09/20/11 <br />Work Order: C11080483 <br />Analytical Run: IC2- C_110812A <br />08/12/11 16:57 <br />Page 18 of 29 <br />08/12/11 17:59 <br />Batch: R149328 <br />08/12/11 17:13 <br />08/12/11 17:28 <br />08/13/11 06:19 <br />