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ENERGY <br />Method: <br />Sample ID: LRB <br />Antimony <br />Arsenic <br />Chromium <br />Copper <br />Iron <br />Lead <br />Manganese <br />Molybdenum <br />Silver <br />Thallium <br />Uranium <br />Zinc <br />E200.8 <br />Sample ID: LFB <br />Antimony <br />Arsenic <br />Chromium <br />Copper <br />Iron <br />Lead <br />Manganese <br />Molybdenum <br />Silver <br />Thallium <br />Uranium <br />Zinc <br />Client: Cotter Corporation <br />Project: Schwartz SW 8/24/11 S25171- S25173 <br />www.energylab.com Helena, Mt 877 - 472 -0711 • Billings, MT 800-735-4489 • Casper, WY 888 -235 -0515 <br />AearyesslEnd ow@ Mu 752 Gillette, WY 866.688 -7175 • Rapid City, SD 888 -672 -1225 • College Station, TX 888 -600 -2218 <br />Analyte <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Qualifiers: <br />RL - Analyte reporting limit. <br />ND - Not detected at the reporting limit. <br />S - Spike recovery outside of advisory limits. <br />12 Method Blank <br />ND mg /L <br />ND mg /L <br />7E -05 mg /L <br />ND mg /L <br />0.0005 mg /L <br />ND mg /L <br />ND mg /L <br />ND mg /L <br />ND mg /L <br />ND mg /L <br />ND mg /L <br />ND mg /L <br />12 Laboratory Fortified Blank <br />0.0522 mg /L <br />0.0525 mg /L <br />0.0500 mg /L <br />0.0518 mg /L <br />1.18 mg /L <br />0.0512 mg /L <br />0.0501 mg /L <br />0.0506 mg /L <br />0.0202 mg /L <br />0.0514 mg /L <br />0.0507 mg /L <br />0.0548 mg /L <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />0.0002 <br />4E -05 <br />5E -05 <br />6E -05 <br />0.0001 <br />2E -05 <br />2E -05 <br />8E -05 <br />8E -05 <br />2E -05 <br />8E -06 <br />0.0001 <br />Run: ICPMS4 -C 110830A <br />Run: ICPMS4 -C 110830A <br />0.0010 104 85 115 <br />0.0010 105 85 115 <br />0.0010 100 85 115 <br />0.0010 104 85 115 <br />0.012 94 85 115 <br />0.0010 102 85 115 <br />0.0010 100 85 115 <br />0.0010 101 85 115 <br />0.0010 101 85 115 <br />0.0010 103 85 115 <br />0.00030 101 85 115 <br />0.0010 110 85 115 <br />Sample ID: 011081096- 002AMS4 12 Sample Matrix Spike Run: ICPMS4- C_110830A <br />Antimony 0.0538 mg /L 0.050 107 70 130 <br />Arsenic 0.0534 mg /L 0.0010 104 70 130 <br />Chromium 0.0597 mg /L 0.050 104 70 130 <br />Copper 0.0521 mg /L 0.010 96 70 130 <br />Iron 1.24 mg /L 0.030 97 70 130 <br />Lead 0.0541 mg /L 0.050 108 70 130 <br />Manganese 0.0566 mg /L 0.010 101 70 130 <br />Molybdenum 0.102 mg /L 0.0010 107 70 130 <br />Silver 0.0120 mg /L 0.010 60 70 130 <br />Thallium 0.0540 mg /L 0.0010 108 70 130 <br />Uranium 0.619 mg /L 0.00030 70 130 <br />Zinc 0.0757 mg /L 0.010 94 70 130 <br />Report Date: 10/05/11 <br />Work Order: 011081023 <br />Batch: R150005A <br />08/30/11 12:07 <br />08/30/11 13:21 <br />08/30/11 21:40 <br />S <br />A <br />Sample ID: C11081096- 002AMSD 12 Sample Matrix Spike Duplicate Run: ICPMS4- C_110830A 08/30/11 21:45 <br />Antimony 0.0543 mg /L 0.050 108 70 130 0.9 20 <br />Arsenic 0.0546 mg /L 0.0010 107 70 130 2.4 20 <br />Chromium 0.0605 mg /L 0.050 105 70 130 1.3 20 <br />Copper 0.0533 mg /L 0.010 99 70 130 2.1 20 <br />A - The analyte level was greater than four times the spike level. In <br />accordance with the method % recovery is not calculated. <br />MDC - Minimum detectable concentration <br />Page 14 of 28 <br />