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A6mZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Sorinos. CO 804871800) 334 -5493 <br />Rhino Energy, LLC ACZ Sample ID: L81585 -02 <br />Project ID: Date Sampled: 04/09/1012:00 <br />Sample ID: TP -4 SAMPLE 2 Date Received: 04114110 <br />Sample Matrix: Soil <br />Soil Analysis <br />EPA Method <br />�Result Qual XQ Units rflDL •Q <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />04/21/10 10:06 <br />me <br />C <br />Method EPA <br />Result Qual <br />XQ <br />Units <br />MDL <br />POL <br />Date <br />Analyst <br />Conductivity @25C <br />SM2510B <br />28.000 <br />M3056B ICP -MS <br />mmhos /cm <br />0.001 <br />0.01 <br />04128/10 16:15 <br />me bsu <br />pH, Saturated Paste <br />USDA No. 60 (21A) <br />8.1 <br />units <br />0.1 <br />0.1 <br />04/28/10 16:15 <br />me bsu <br />Saturation Percent <br />USDA No. 60 (2) <br />103 <br />% <br />0.01 <br />0.1 <br />04/28/10 16:15 <br />me bsu <br />Sulfur Forms <br />M600/2- 78-054 3.2.4 -MOD <br />Sulfur HCI Residue <br />1.03 <br />% <br />0.01 <br />0.1 <br />04/28/10 0:00 <br />bsu <br />Sulfur HNO3 Residue <br />0.65 <br />% <br />0.01 <br />0.1 <br />04/28/10 0:00 <br />bsu <br />Sulfur Organic <br />0.65 <br />* <br />% <br />0.01 <br />0.1 <br />04/28110 0:00 <br />bsu <br />Residual Mod <br />Sulfur Pyritic Sulfide <br />0.38 <br />% <br />0.01 <br />0.1 <br />04/28/10 0:00 <br />bsu <br />Sulfur Sulfate <br />1.17 <br />% <br />0.01 <br />0.1 <br />04128/10 0:00 <br />bsu <br />Sulfur Total <br />2.20 <br />% <br />0.01 <br />0.1 <br />04/28/10 0:00 <br />bsu <br />Total Sulfur minus <br />1.03 <br />% <br />0.01 <br />0.1 <br />04/28/10 0:00 <br />bsu <br />Sulfate <br />Texture by Hydrometer <br />ASTM D 422 Hydrometer <br />Clay <br />23.8 <br />* <br />% <br />0.1 <br />0.5 <br />04/29/10 0:00 <br />brd /bsu <br />Sand <br />61.3 <br />* <br />% <br />0.1 <br />0.5 <br />04/29/10 0:00 <br />brd/bsu <br />Silt <br />15.0 <br />* <br />% <br />0.1 <br />0.5 <br />04/29/10 0:00 <br />brd/bsu <br />Texture Classification <br />Sandy Clay <br />* <br />04/29/10 0:00 <br />brd/bsu <br />Loam <br />Total Solids <br />SM2540B <br />72.90 <br />% <br />0.01 <br />0.1 <br />04/22/10 0:30 <br />me <br />Total Volatile Solids <br />M2540G, Gravimetric <br />64.80 <br />% <br />0.01 <br />0.1 <br />04122/10 0:30 <br />me <br />ti <br />Soil Preparation <br />Parameter <br />EPA Method <br />�Result Qual XQ Units rflDL •Q <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />04/21/10 10:06 <br />me <br />C <br />Crush and Pulverize <br />USDA No. 1, 1972 <br />04/27/10 11:23 <br />me <br />Digestion - Hot Plate <br />M3050B ICP <br />04/28/1013:32 <br />bsu <br />Digestion - Hot Plate <br />M3056B ICP -MS <br />04/28/10 13:32 <br />bsu <br />Saturated Paste <br />USDA No. 60 (2) <br />04/28/10 13:51 <br />me bsu <br />Extraction <br />Water Extraction <br />ASA No. 9 10- 2.3.2 <br />04/28/10 22:14 <br />bsu <br />Wet Chemistry <br />Parameter EPA Method. Result Qual XQ ]'�Units MDL POL Date Analyst <br />Nitrate /Nitrite as N, M353.2 -Automated Cadmium 99 * mg /Kg 2 10 04/29/10 22:14 pib <br />soluble (Water) Reduction <br />REPIN.02.06.05.01 <br />* Please refer to Qualifier Reports for details. <br />Page 6 of 21 <br />