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16iZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Sodnas. CO 80487(800) 334 -5493 <br />Rhino Energy, LLC ACZ Sample ID: L81585 -01 <br />Project ID: Date Sampled: 04109110 11:21 <br />Sample ID: TP -3 SAMPLE 2 Date Received: 04114110 <br />Sample Matrix: Soil <br />Soil Preparation <br />Wet Chemistry <br />Method Parameter EPA Result Qual X0 Units MDL POL Date Analyst <br />Nitrate /Nitrite as N, M353.2 - Automated Cadmium 290 mg/Kg 10 50 04/29/10 22:06 pjb <br />soluble (Water) Reduction <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 4 of 21 <br />Q 'Q Inits F1JDL •• <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />04/21/10 10:00 <br />me <br />C <br />Crush and Pulverize <br />USDA No. 1, 1972 <br />04/27/10 11 :00 <br />me <br />Digestion - Hot Plate <br />M3050B ICP <br />04/28/10 12:35 <br />bsu <br />Digestion - Hot Plate <br />M3050B ICP -MS <br />04/28/10 12:35 <br />bsu <br />Saturated Paste <br />USDA No. 60 (2) <br />04/2811011:00 <br />me bsu <br />Extraction <br />Water Extraction <br />ASA No. 9 10- 2.3.2 <br />04/28/10 17:52 <br />bsu <br />Wet Chemistry <br />Method Parameter EPA Result Qual X0 Units MDL POL Date Analyst <br />Nitrate /Nitrite as N, M353.2 - Automated Cadmium 290 mg/Kg 10 50 04/29/10 22:06 pjb <br />soluble (Water) Reduction <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 4 of 21 <br />