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I ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Snnnos. CO 80487 /800) 334 -5493 <br />Rhino Energy, LLC ACZ Sample ID: L81711 -03 <br />Project ID: Date Sampled: 04119110 12:33 <br />Sample ID: TP -3 SAMPLE 3 Date Received: 04121110 <br />Sample Matrix: Soil <br />Soil Preparation <br />Parameter <br />EPA Method <br />Result Qual AQ Inits F11L)L PIEL k. - Analyst <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />04123/10 15:50 <br />me <br />C <br />Crush and Pulverize <br />USDA No. 1, 1972 <br />04127/10 17:36 <br />me <br />Digestion - Hot Plate <br />M3050B ICP <br />04/28/10 17:02 <br />bsu <br />Digestion - Hot Plate <br />M3050B ICP -MS <br />04128/10 17:02 <br />bsu <br />Saturated Paste <br />USDA No. 60 (2) <br />05/03/10 14:36 <br />me <br />Extraction <br />Water Extraction <br />ASA No. 9 10 -2.3.2 <br />05/04/10 13:22 <br />bsu <br />Wet Chemistry <br />Method Resu It XQ Units MDL POL Date Analyst <br />Nitrate/Nitrite as N, M353.2 - Automated Cadmium 140 mg /Kg 1 5 05/05/10 23:35 pjb <br />soluble (Water) Reduction <br />REPIN.02.06.05.01 ` Please refer to Qualifier Reports for details. <br />Page 8 of 20 <br />