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ENERGY <br />RZ•1 h - _S <br />Client: Cotter Corporation <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energylab corn <br />Analytical Easilesc.awe 1852 <br />J <br />Helena, Mr 877472 -0711 • Billings, MT 808 - 735 -4489 • Casper, WY 888- 235 -0515 <br />Gillette, WY 866- 686 -7175 • Rapid City, SD 888- 672 -1225 • College Station, TX 888 -690 -2218 <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch <br />Report Date: 01/30/12 <br />Project: Schwartz GW 12/29/11 S26170- S26171 Work Order: 011120864 <br />I <br />Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.8 Analytical Run: ICPMS4- C_120103A <br />Sample ID: ICV 3 Initial Calibration Verification Standard 01/03/12 13:24 <br />Copper 0 0495 mg /L 0.0010 99 90 110 <br />Iron 0.995 mg /L 0.0010 99 90 110 <br />Zinc 0.0500 mg /L 0.0010 100 90 110 <br />Method: E200.8 Batch: R154993A <br />Sample ID: LRB 3 Method Blank Run: ICPMS4- C_120103A 01/03/12 22:35 <br />Copper ND mg /L 0.0010 <br />Iron ND mg /L 0.030 <br />Zinc ND mg /L 0.0050 <br />Sample ID: LFB 3 Laboratory Fortified Blank Run: ICPMS4- C_120103A 01/03/12 22:42 <br />Copper 0 0508 mg /L 0.0010 102 85 115 <br />Iron 1.20 mg /L 0.0010 96 85 115 <br />Zinc 0.0526 mg /L 0.0010 104 85 115 <br />Sample ID: C11120668- 001BMS4 3 Sample Matrix Spike Run: ICPMS4- C_120103A 01/04/12 21:29 <br />Copper 0.0479 mg /L 0.010 95 70 130 <br />Iron 1.16 mg /L 0.030 92 70 130 <br />Zinc 0.0535 mg /L 0.010 92 70 130 <br />Sample ID: C11120668- 001BMSD 3 Sample Matrix Spike Duplicate Run: ICPMS4- C_120103A 01/04/12 21:36 <br />Copper 0.0483 mg /L 0 010 96 70 130 0.8 20 <br />Iron 120 mg /L 0.030 96 70 130 3.9 20 <br />Zinc 0.0554 mg /L 0.010 96 70 130 3.5 20 <br />ND - Not detected at the reporting limit. <br />Page 12 of 24 <br />