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ENERGY <br />Qualifiers: <br />1 <br />Method: E300.0 <br />Sample ID: ICV092711 -10 <br />Chloride <br />Sulfate <br />www.energylab.com <br />Assildw/Eteabety Saco 1852 <br />Client: Cotter Corporation <br />Project: Schwartz GW 9/22/11 S26016 <br />Helene, MT 877472 -0711 • Billings, MT 600 -735 -4489 • Gasper, WY 888- 235 -0515 <br />Gillette, WY 866 -686 -7175 • Rapid City, SO 888 - 672 -1225 • college Station, TX 888- 690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />2 Initial Calibration Verification Standard <br />10.2 mg /L <br />41.3 mg /L <br />Method: E300.0 <br />Sample ID: ICB092711 -11 2 Method Blank <br />Chloride ND mg /L 0.10 <br />Sulfate 0.3 mg /L 0.08 <br />1.0 102 90 110 <br />1.0 103 90 110 <br />Run: IC2 -C 110927B <br />Sample ID: LFB092711 -12 2 Laboratory Fortified Blank Run: IC2- C_110927B <br />Chloride 9.94 mg /L 1.0 99 90 110 <br />Sulfate 40.3 mg /L 1.0 100 90 110 <br />Sample ID: 011090952- 009AMS 2 Sample Matrix Spike Run: IC2- C_110927B <br />Chloride 22.2 mg /L 1.0 101 90 110 <br />Sulfate 415 mg /L 1.6 90 110 <br />Report Date: 10/31/11 <br />Work Order: C11090956 <br />Analyte <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Analytical Run: IC2- C_110927B <br />09/27/11 15:33 <br />Page 12 of 20 <br />Batch: R151305 <br />09/27/11 15:49 <br />09/27/11 16:04 <br />09/29/11 11:26 <br />A <br />Sample ID: C11090952- 009AMSD 2 Sample Matrix Spike Duplicate Run: IC2- C_110927B 09/29/11 11:41 <br />Chloride 22.5 mg /L 1.0 103 90 110 1.2 10 <br />Sulfate 414 mg /L 1.6 90 110 0.3 10 A <br />RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In <br />accordance with the method % recovery is not calculated. <br />ND - Not detected at the reporting limit. MDC - Minimum detectable concentration <br />