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ENERGY <br />Method: E200.8 <br />Sample ID: MB -30670 <br />Antimony <br />Arsenic <br />Chromium <br />Copper <br />Iron <br />Lead <br />Manganese <br />Molybdenum <br />Silver <br />Thallium <br />Uranium <br />Zinc <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energylab.com <br />Analytical Ercelemp sace 1152 <br />Client: Cotter Corporation <br />Project: Schwartz SW 8/2/11 S25901- S25908 <br />12 Method Blank <br />ND mg /L <br />0.003 mg /L <br />0.002 mg /L <br />0.003 mg /L <br />0.005 mg /L <br />ND mg /L <br />0.0010 mg /L <br />ND mg /L <br />5E -05 mg /L <br />ND mg /L <br />ND mg /L <br />ND mg /L <br />Helena, MT 877- 472 -0711 • Billings, MT 800- 735 -4489 • Casper, WY 888 -235 -0515 <br />Gillette, WY 866 -686 -7175 • Rapid City, SD 888 - 672 -1225 • College Station, TX 888 -690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Analyte <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />0.0003 <br />5E -05 <br />3E -05 <br />5E -05 <br />0.001 <br />5E -05 <br />2E -05 <br />0.00010 <br />4E -05 <br />0.0001 <br />4E -05 <br />0.001 <br />Run: ICPMS4- C_110808A <br />Sample ID: LCS3 -30670 12 Laboratory Control Sample Run: ICPMS4- C_110808A <br />Antimony 0.561 mg /L 0.050 112 85 115 <br />Arsenic 0.527 mg /L 0.0010 105 85 115 <br />Chromium 0.552 mg /L 0.050 110 85 115 <br />Copper 0.517 mg /L 0.010 103 85 115 <br />Iron 2.51 mg /L 0.030 100 85 115 <br />Lead 0 546 mg /L 0.050 109 85 115 <br />Manganese 2.64 mg /L 0.010 106 85 115 <br />Molybdenum 0.545 mg /L 0.10 109 85 115 <br />Silver 0.0547 mg /L 0.010 109 85 115 <br />Thallium 0.537 mg /L 0.10 107 85 115 <br />Uranium 0.550 mg /L 0.00030 110 85 115 <br />Zinc 0.521 mg /L 0.010 104 85 115 <br />Sample ID: C11080157- 008DMS3 12 Sample Matrix Spike Run: ICPMS4- C_110808A 08/08/11 17:19 <br />Antimony 0.570 mg /L 0.050 114 70 130 <br />Arsenic 0.496 mg /L 0.0010 99 70 130 <br />Chromium 0.518 mg /L 0.050 103 70 130 <br />Copper 0.494 mg /L 0.010 98 70 130 <br />Iron 2.76 mg /L 0.030 96 70 130 <br />Lead 0.544 mg /L 0.050 109 70 130 <br />Manganese 2.64 mg /L 0.010 105 70 130 <br />Molybdenum 0.549 mg /L 0.10 109 70 130 <br />Silver 0.0537 mg /L 0.010 107 70 130 <br />Thallium 0 536 mg /L 0.10 107 70 130 <br />Uranium 0.566 mg /L 0.00030 109 70 130 <br />Zinc 0.496 mg /L 0.010 98 70 130 <br />Sample ID: C11080157- 008DMSD 12 Sample Matrix Spike Duplicate Run: ICPMS4- C_110808A 08/08/11 17:23 <br />Antimony 0.548 mg /L 0.050 110 70 130 3.9 20 <br />Arsenic 0.479 mg /L 0.0010 95 70 130 3.5 20 <br />ND - Not detected at the reporting limit. <br />Report Date: 09/13/11 <br />Work Order: C11080157 <br />Page 21 of 41 <br />Batch: 30670 <br />08/08/11 15:53 <br />08/08/11 15:57 <br />