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• 5. Yoast Mine Spoil Sampling (December 2004) — 4 randomly distributed locations at <br />the Yoast Mine were sampled for regraded spoil. Mr. Roy Karo of Seneca Coal <br />Company collected the samples. They were subsequently sent to CSU for analysis. <br />The samples were numbered YSTRS -03 -01 through YSTRS- 03 -04. The attached <br />map shows all sample locations. <br />2.0 Methods <br />Each area to be sampled was delineated on a Seneca photobase map. All sample <br />locations were randomly distributed across each area. All locations were sampled by tile <br />spade and soil auger. A composite sample of the appropriate depth interval was collected <br />at each location. Samples were screened in the field over a No. 10 (2mm) screen to <br />remove hard rocks. Sample depth was noted for each location as well as other <br />information if pertinent. Soil backhoe pits were located and dug by Seneca. In addition <br />to soil sampling, a complete soil profile description was completed at each backhoe pit <br />location. Soils description followed standard Natural Resources Conservation Service <br />(MRCS) field methods (Schoenberger et.al., 2002). Digital photographs were taken of <br />each pit and adjacent landscape. All soil and spoil laboratory data was reviewed and <br />approved by CSU Laboratory Director Mr. Jim Self. Jim Nyenhuis also reviewed the <br />data and requested several reruns for confirmation purposes. <br />All soil and spoil samples were analyzed by CSU. The soil fertility parameters included: <br />• pH; electrical conductivity (EC); organic matter percent (Walkley -Black method); time <br />estimate; texture estimate; and several nutrients and micronutrients (ppm by AB -DTPA <br />Extract) including nitrate nitrogen (NO3 -N), phosphorus (P), potassium (K), zinc (Zn), <br />iron (Fe), manganese (Mn), and copper (Cu). <br />Overburden spoil parameters included: pH; electrical conductivity (EC); particle size <br />(percent sand, silt, and clay by hydrometer), boron (B), acid -base potential (A:B <br />potential), saturation percent; the same nutrients and micronutrients as for soil; and <br />sodium adsorption ratio (SAR) which is calculation requiring meq/L, of calcium (Ca), <br />magnesium (Mg), sodium (Na), and potassium (K). <br />All field and laboratory data was evaluated for suitability based on standard threshold <br />values for significant parameters, primarily EC, SAR, AB potential, and B (WDEQ, <br />1994). <br />3.0 Results <br />Soil and Overburden Spoil Laboratory Results <br />Four sets of laboratory data are attached to this report. Set 1 was reported on August 13, <br />2004 and includes the 25 topsoils sampled in June from 2W as well as 2 samples from the <br />2W topsoil backhoe pit #1; and the 25 topsoils sampled in June from Yoast as well as 6 <br />• samples from Yoast topsoil backhoe pits #1 and 2. Set 2 was reported on August 27, <br />2004 and includes the 25 regraded spoils sampled in June from 2W. Set 3 was reported <br />