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S G$ <br />October 17, 2011 <br />New Elk Coal Company <br />122 West First St. <br />Trinidad, CO 81082 <br />USA <br />Client Sample ID: <br />Date Received: <br />Matrix: <br />TESTS <br />Alkalinity, Total <br />Conductivity <br />Hardness, Calculated Total <br />Mercury, Total <br />Calcium, Dissolved <br />Magnesium, Dissolved <br />Sodium, Dissolved <br />Lead, Potentially Dissolved <br />Selenium, Potentially Dissolved <br />Silver, Potentially Dissolved <br />Cadmium, Potentially Dissolved <br />Copper, Potentially Dissolved <br />Manganese, Potentially Dissolved <br />Nickel, Potentially Dissolved <br />Zinc, Potentially Dissolved <br />Arsenic, Total <br />Boron, Total <br />Iron, Total <br />Aluminum, Total Recoverable <br />Chromium, Total Recoverable <br />Iron, Total Recoverable <br />Nitrogen, Ammonia <br />pH <br />pH Temperature <br />Sodium Absorption Ratio <br />Solids, Total Suspended <br />Pond #1 <br />01/27/2010 <br />Water <br />SGS Minerals Sample ID: 072 - 43620 -001 <br />RESULT <br />1300 mg /L CaCO3 <br />2200 umhos/cm <br />46 mg/L CaCO3 <br /><0.2 ug/L <br />10 mg /L <br />4.9 mg/L <br />610 mg /L <br /><0.005 mg/L <br /><0.002 mg /L <br /><0.0005 mg /L <br /><0.005 mg /L <br /><0.005 mg /L <br />0.012 mg /L <br /><0.01 mg /L <br />0.005 mg /L <br /><0.002 mg /L <br />0.03 mg/L <br />0.05 mg /L <br /><0.02 mg /L <br /><0.005 mg /L <br />0.05 mg /L <br />1.5 mg /L N <br />7.60 s.u. <br />16.5 °C <br />39 <br /><5 mg/L <br />Analysis Report <br />Date Sampled : <br />Kind of Sample : <br />Project Name /# : <br />Sample Taken By : <br />Time Sampled : <br />01/26/2010 <br />GW <br />New Elk Mine <br />R. Thompson <br />1300 <br />Page 1 of 2 <br />REPORTING ANALYZED <br />METHOD LIMIT DATE / TIME ANALYST <br />SM2320 B 1 02/03/2010 1445 SV <br />SM2510 B 1 01/27/2010 2010 SV <br />Calc 1 <br />EPA245.1 0.2 02/03/2010 1000 DAH <br />EPA200.7 0.01 01/28/2010 1900 EH <br />EPA200.7 0.01 01/28/2010 1900 EH <br />EPA200.7 0.05 01/28/2010 1900 EH <br />EPA200.7 0.005 01/28/2010 1800 EH <br />EPA200.9 0.002 02/05/2010 1750 EH <br />EPA200.7 0.0005 01/28/2010 1800 EH <br />EPA200.7 0.005 01/28/2010 1800 EH <br />EPA200.7 0.005 01/28/2010 1800 EH <br />EPA200.7 0.005 01/28/2010 1800 EH <br />EPA200.7 0.01 01/28/2010 1800 EH <br />EPA200.7 0.005 01/28/2010 1800 EH <br />EPA200.9 0.002 02/05/2010 1250 EH <br />EPA200.7 0.02 02/05/2010 1720 EH <br />EPA200.7 0.01 02/05/2010 1720 EH <br />EPA200.7 0.02 02/05/2010 1655 EH <br />EPA200.7 0.005 02/05/2010 1655 EH <br />EPA200.7 0.01 02/05/2010 1655 EH <br />SM4500 -NH3 H 0.05 02/03/2010 0900 SV <br />SM4500 -H B 0.01 01/27/2010 1345 SV <br />SM4500 -H B 01/27/2010 1345 SV <br />Calc 0.01 <br />SM2540 D 5 02/02/2010 1350 SV <br />714'' Somer Rodriguez, Denver Laboratory <br />SOS North America ho. I Minerals Services Oiiison <br />4665 Paris St Suite B -200 Denver CO 80239 t (303)373.4772 f (303)373 -4791 www.sgs,comininerals <br />Memberof SGS Group <br />This document is Issued by the Company under its General Conditions of Service accessible at http:// www .sgs.com/lerms_and_conditans.htm Attention is <br />drawn to the limitation of liability, indemnification and jurisdiction issues defined Merin. <br />Any holder of this document is advised that information contained hereon reflects the Company's findings at the time of its intervention only and within the limits <br />of Client's instructions, if any. The Company's sole responsibility is to its client and this document does not exonerate parties to a transaction from exercising all <br />their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document <br />is unlawful and offenders may be prosecuted to the fullest extent of the law. <br />