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SG$ <br />October 17, 2011 <br />New Elk Coal Company <br />122 West First St. <br />Trinidad, CO 81082 <br />USA <br />Client Sample ID: <br />Date Received: <br />Matrix: <br />TESTS <br />Alkalinity, Total <br />Conductivity <br />Hardness, Calculated Total <br />Mercury, Total <br />Calcium, Dissolved <br />Magnesium, Dissolved <br />Sodium, Dissolved <br />Lead, Potentially Dissolved <br />Selenium, Potentially Dissolved <br />Silver, Potentially Dissolved <br />Cadmium, Potentially Dissolved <br />Copper, Potentially Dissolved <br />Manganese, Potentially Dissolved <br />Nickel, Potentially Dissolved <br />Zinc, Potentially Dissolved <br />Arsenic, Total <br />Boron, Total <br />Iron, Total <br />Aluminum, Total Recoverable <br />Chromium, Total Recoverable <br />Iron, Total Recoverable <br />Nitrogen, Ammonia <br />pH <br />pH Temperature <br />Sodium Absorption Ratio <br />Solids, Total Suspended <br />Pond #1 <br />01/08/2010 <br />Water <br />Analysis Report <br />Date Sampled : <br />Project Name /# : <br />Sample Taken By : <br />Time Sampled : <br />SGS Minerals Sample ID: 072-43289-001 <br />RgSULT <br />1400 mg /L CaCO3 <br />2300 umhos/cm <br />48 mg /L CaCO3 <br /><0.2 ug/L <br />11 mg/L <br />5.2 mg/L <br />670 mg /L <br /><0.005 mg/L <br /><0.002 mg/L <br /><0.0005 mg/L <br /><0.005 mg/L <br /><0.005 mg/L <br />0.013 mg/L <br /><0.01 mg/L <br /><0.005 mg/L <br /><0.002 mg /L <br />0.03 mg/L <br />0.06 mg/L <br /><0.02 mg /L <br /><0.005 mg /L <br />0.03 mg /L <br />1.6 mg /L N <br />7.65 s.u. <br />17.5 °C <br />42 <br /><5 mg /L <br />REPORTING <br />METHOD LIMIT <br />01/05/2010 <br />Pond #1 <br />Bobby Steele <br />1:30 PM <br />Page 1 of 2 <br />ANALYZED <br />DATE / TIME ANALYST <br />SM2320 B 1 01/19/2010 1115 DM <br />SM2510 B 1 01/14/2010 1145 DM <br />Calc 1 <br />EPA245.1 0.2 <br />EPA200.7 0.01 <br />EPA200.7 0.01 <br />EPA200.7 0.05 <br />EPA200.7 0.005 <br />EPA200.9 0.002 <br />EPA200.7 0.0005 <br />EPA200.7 0.005 <br />EPA200.7 0.005 <br />EPA200.7 0.005 <br />EPA200.7 0.01 <br />EPA200.7 0.005 <br />EPA200.9 0.002 <br />EPA200.7 0.02 <br />EPA200.7 0.01 <br />EPA200.7 0.02 <br />EPA200.7 0.005 <br />EPA200.7 0.01 <br />SM4500 -NH3 H 0.05 <br />SM4500 -H B 0.01 <br />SM4500 -H B <br />Calc 0.01 <br />SM2540 D 5 01/12/2010 1200 ST <br />01/13/2010 1100 DAH <br />01/12/2010 1230 EH <br />01/12/2010 1230 EH <br />01/12/2010 1230 EH <br />01/12/2010 1730 EH <br />01/19/2010 1400 SK <br />01/12/2010 1730 EH <br />01/12/2010 1730 EH <br />01/12/2010 1730 EH <br />01/12/2010 1730 EH <br />01/12/2010 1730 EH <br />01/12/2010 1730 EH <br />01/19/2010 1300 SK <br />01/12/2010 1800 EH <br />01/12/2010 1800 EH <br />01/14/2010 1200 EH <br />01/14/2010 1200 EH <br />01/14/2010 1200 EH <br />01/13/2010 0830 ST <br />01/08/2010 1330 SV <br />01/08/2010 1330 SV <br />Sourer Rodriguez, Denver Laboratory <br />SGS North America hc. Mnerals Services Division <br />4883 Paris St Suite 8 -200 Denver CO 80239 t (303)373.4772 f (303)373.4791 wwwsgscomininerals <br />tufemberof SOS Group <br />This document is Issued by the Company under its General Conditions of Service accessible at http: / /www.sgs.com/terms and_conditions.htm Attention is <br />drawn to the limitation of liability, indemnification and jurisdiction issues defined therin. <br />Any holder of this document is advised that information contained hereon reflects the Company's findings at the time of its intervention only and within the limits <br />of Client's instructions, if any. The Company's sole responsibility is to its client and this document does not exonerate parties to a transaction from exercising all <br />their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document <br />is unlawful and offenders may be prosecuted to the fullest extent of the law. <br />