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TDS <br />TDS <br />TDS <br />GCC Energy, LLC <br />6473 CR 120 <br />Hesperus CO, 81326 <br />Project: Quarterly <br />Project Name / Number: King I & King II <br />Project Manager: Tom Bird <br />Reported: <br />10/12/11 09:53 <br />Analyte <br />Result <br />Reporting Spike Source %REC RPD <br />Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch B110040 - General Prep - Wet Chem <br />Blank (B110040 -BLK1) <br />Duplicate (B110040 -DUP1) <br />Reference (B110040 -SRMI ) <br />Batch B110072 - General Prep - Wet Chem <br />Blank (B110072 -BLK1) <br />Sulfate <br />LCS (B110072 -BSI) <br />Analytical <br />Laboratories <br />dzufelt@greenanalytical.com p: 970.247.4220 f: 970.247.4227 75 Suttle Street Durango, CO 81303 <br />General Chemistry - Quality Control <br />ND 10.0 mg/L <br />Source: 1110007 - 01 Prepared & Analyzed: 10 /04/11 <br />185 10.0 mg/L <br />3420 10.0 mg/L 3510 97.4 85 -115 <br />ND 10.0 mg/L <br />Prepared & Analyzed: 10 /04/11 <br />210 <br />Prepared & Analyzed: 10 /04/11 <br />Prepared & Analyzed: 10 /08/11 <br />Prepared & Analyzed: 10/08/11 <br />Sulfate 54.0 10.0 mg/L 50.0 108 80 - 120 <br />LCS Dup (B110072 - BSD1) Prepared & Analyzed: 10/08/11 <br />Sulfate 55.0 10.0 mg/L 50.0 110 80 - 120 1.83 20 <br />Batch B110075 - General Prep - Wet Chem <br />Duplicate (B110075 -DUPS) <br />Source: 1110008 -01 Prepared & Analyzed: 10 /03/11 <br />PH 7.41 pH Units 7.13 3.85 20 <br />Reference (B110075 Prepared & Analyzed: 10 /03/11 <br />pH 8.26 pH Units 8.30 99.5 90 -110 <br />Green Analytical Laboratories <br />fo_tattx:,4,3,44- <br />Debbie Zufelt, Reports Manager <br />www.GreenAnalytical.com <br />12.7 20 <br />The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirety. In no event <br />shall Green Analytical Laboratories be liable for incidental or consequential damages. <br />GALs liability, and clients exclusive remedy for any claim arising, shall be limited to the <br />amount paid by client for analyses. All claims, including those for negligence and any other <br />cause whatsoever, shall be deemed waived unless made in writing and received within <br />thirty days after completion of the applicable service. <br />I Page 7of11 I <br />